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CAS No. : | 1095822-37-9 | MDL No. : | MFCD20660139 |
Formula : | C7H6N4O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | N/A |
M.W : | 178.15 | Pubchem ID : | - |
Synonyms : |
|
TPSA :Topological Polar Surface Area | - | H-Bond Acceptor Count : | - |
XLogP3 : | - | H-Bond Donor Count : | - |
SP3 : | - | Rotatable Bond Count : | - |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Synthesis of compound 8. A solution of 1M of LiOH (3.6 mL) was added to a solution compound 8.1 (850 mg, 3.6 mmol) in THF (20 mL). After the reaction was complete, the solvent was removed. The residue was taken up in MeOH and 4M hydrogen chloride in 1,4-dioxane (0.646 mL) was added. Concetration of the mixture provided 8. 1H-NMR (400.13 MHz, DMSO-d6) δ=8.83 (s, 1H), 8.56 (s, 1H), 3.84 (s, 3H). |
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