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CAS No. : | 111-77-3 | MDL No. : | MFCD00002871 |
Formula : | C5H12O3 | Boiling Point : | - |
Linear Structure Formula : | HO(C2H4O)2CH3 | InChI Key : | SBASXUCJHJRPEV-UHFFFAOYSA-N |
M.W : | 120.15 | Pubchem ID : | 8134 |
Synonyms : |
|
Chemical Name : | 2-(2-Methoxyethoxy)ethanol |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P201-P202-P210-P280-P308+P313-P370+P378-P403+P235-P405-P501 | UN#: | N/A |
Hazard Statements: | H227-H361 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
6.9 g | With di(n-butyl)tin oxide; In toluene; for 8h;Dean-Stark; Reflux; | In a reaction vessel equipped with a Dean-Stark apparatus, 5.0 g of a compound represented by the formula (I-3-1)3.9 g of the compound represented by the formula (I-3-2), 0.1 g of dibutyltin oxide,90 mL of toluene was added, and the mixture was heated under reflux for 8 hours while changing toluene. After distilling off toluene, it was purified by column chromatography (silica gel, ethyl acetate / hexane) to obtain 6.9 g of a compound represented by the formula (I-3-3). |
6.9 g | With di(n-butyl)tin oxide; In toluene; for 8h;Dean-Stark; Reflux; | 5.0 g of the compound represented by the formula (I-3-1) in a reaction vessel equipped with a Dean-Stark apparatus. , 3.9 g of the compound represented by the formula (I-3-2), 0.1 g of dibutyltin oxide, tolue 90 mL was added, and the mixture was heated under reflux for 8 hours while replacing toluene. Distill off toluene After that, purification is performed by column chromatography (silica gel, ethyl acetate / hexane). No, 6.9 g of the compound represented by the formula (I-3-3) was obtained. |
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