Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | |||||
{[ item.p_purity ]} | {[ item.pr_size ]} |
{[ getRatePrice(item.pr_usd, 1,1) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate) ]} |
{[ getRatePrice(item.pr_usd, 1,1) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate) ]} | {[ item.pr_usastock ]} | Inquiry - | {[ item.pr_chinastock ]} | Inquiry - |
* Storage: {[proInfo.prStorage]}
CAS No. : | 531521-23-0 | MDL No. : | MFCD30531305 |
Formula : | C10H20O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 204.26 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70% | With sodium hydride; In tetrahydrofuran; at 0 - 20℃; for 48h; | Diethylene glycol monomethyl ether (20g, 170mmol) and sodium hydride (4g, 170mmol) in anhydrous tetrahydrofuran until no bubbles, and then at 0 3- (methyl tosylate) oxy oxetane (41.2g, 170mmol) was added dropwise to the reaction system, the reaction was added dropwise at room temperature 48 hours after recovery.After the reaction, the reaction solution was diluted with water and extracted by dichloromethane, distilled under reduced pressure to give a colorless liquid.Yield: 70% |