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Chemistry
Heterocyclic Building Blocks
Pyridines
Ethyl 6-chloro-4-methoxypicolinate
Chemistry
Heterocyclic Building Blocks
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Chlorides Esters Ethers

[ CAS No. 1122090-80-5 ] {[proInfo.proName]}

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Chemical Structure| 1122090-80-5
Chemical Structure| 1122090-80-5
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COA NMR CNMR HPLC LC-MS

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Product Details of [ 1122090-80-5 ]

CAS No. :1122090-80-5 MDL No. :MFCD18416483
Formula : C9H10ClNO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 215.63 Pubchem ID :-
Synonyms :

Safety of [ 1122090-80-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1122090-80-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1122090-80-5 ]

[ 1122090-80-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 88912-21-4 ]
  • [ 64-17-5 ]
  • [ 1122090-80-5 ]
YieldReaction ConditionsOperation in experiment
With chloro-trimethyl-silane; at 20℃; for 16h; To a stirred solution of <strong>[88912-21-4]6-chloro-4-methoxypyridine-2-carboxylic acid</strong> (5.00 g, 26.7 mmol) in ethanol (75 ml_), chlorotrimethylsilane (15 ml_) is added. The reaction mixture is stirred at rt for 16 h before the solvent is evaporated. The remaining residue is dried under vacuum to give 6-chloro-4-methoxy-2-carboxylic acid ethyl ester (5.95 g) as a pale yellow oil; LC-MS: tR = 0.85 min; [IVM]+ = 215.97; 1H NMR (CDCI3): delta lambda AA (t, J = 7.0 Hz, 3 H), 3.94 (s, 3 H), 4.48 (q, J = 7.0 Hz, 2 H), 7.01 (d, J = 2.0 Hz, 1 H), 7.61 (d, J = 2.0 Hz, 1 H).
With chloro-trimethyl-silane; at 20℃; for 16h; a) To a stirred solution of <strong>[88912-21-4]6-chloro-4-methoxypyridine-2-carboxylic acid</strong> (5.00 g, 26.7 mmol) in ethanol (75 mL), chlorotrimethylsilane (15 mL) is added. The reaction mixture is stirred at rt for 16 h before the solvent is evaporated. The remaining residue is dried under vacuum to give 6-chloro-4-methoxy-2-carboxylic acid ethyl ester (5.95 g) as a pale yellow oil; LC-MS: tR=0.85 min; [M+1]+=215.97; 1H NMR (CDCl3): delta 1.44 (t, J=7.0 Hz, 3H), 3.94 (s, 3H), 4.48 (q, J=7.0 Hz, 2H), 7.01 (d, J=2.0 Hz, 1H), 7.61 (d, J=2.0 Hz, 1H).
With chloro-trimethyl-silane; at 20℃; for 16h; To a stirred solution of <strong>[88912-21-4]6-chloro-4-methoxypyridine-2-carboxylic acid</strong> (5.00 g, 26.7 mmol) in ethanol (75 mL), chlorotrimethylsilane (15 mL) is added. The reaction mixture is stirred at rt for 16 h before the solvent is evaporated. The remaining residue is dried under vacuum to give 6-chloro-4-methoxy-2-carboxylic acid ethyl ester (5.95 g) as a pale yellow oil; LC- MS: tR = 0.85 min; [M+1]+ = 215.97; 1H NMR (CDCI3): delta 1.44 (t, J = 7.0 Hz, 3 H), 3.94 (s, 3 H), 4.48 (q, J = 7.0 Hz, 2 H), 7.01 (d, J = 2.0 Hz, 1 H), 7.61 (d, J = 2.0 Hz, 1 H).
Reference： [1]Patent: WO2009/24905,2009,A1 .Location in patent: Page/Page column 77
[2]Patent: US2011/212998,2011,A1 .Location in patent: Page/Page column 28
[3]Patent: WO2009/109872,2009,A1 .Location in patent: Page/Page column 30

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