Home Cart 0 Sign in  

[ CAS No. 113853-92-2 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 113853-92-2
Chemical Structure| 113853-92-2
Structure of 113853-92-2 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 113853-92-2 ]

Related Doc. of [ 113853-92-2 ]

Alternatived Products of [ 113853-92-2 ]

Product Details of [ 113853-92-2 ]

CAS No. :113853-92-2 MDL No. :MFCD07369339
Formula : C10H14BrNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 260.13 Pubchem ID :-
Synonyms :

Safety of [ 113853-92-2 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 113853-92-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 113853-92-2 ]

[ 113853-92-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17608-10-5 ]
  • [ 113853-92-2 ]
  • [ 138977-28-3 ]
YieldReaction ConditionsOperation in experiment
79% With triethylamine In tetrahydrofuran for 18h;
70% With triethylamine In N,N-dimethyl-formamide at 20℃; for 4h;
With triethylamine In DMF (N,N-dimethyl-formamide) for 65h; 10 The hydrobromic salt of the bicyclic amine (1 eq.) was dissolved in DMF and triethylamine (3 eq.) was added. This mixture was stirred for 15-30 minutes and then was the isothiocyanate (1.2 eq.) added. This mixture was stirred for 65 hours and then concentrated. The residue was dissolved in EtOAc and washed with water. The organic phase was dried (MgSO4) and concentrated to give the crude product, typically as a yellow oil. The thiourea was chromatographed on silicagel (heptane:EtOAc). The substituted thioureas thus prepared are listed in Table 5.
Same Skeleton Products
Historical Records