Home Cart Sign in  
Chemical Structure| 1140-16-5 Chemical Structure| 1140-16-5

Structure of 1140-16-5

Chemical Structure| 1140-16-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1140-16-5 ]

CAS No. :1140-16-5
Formula : C15H14O
M.W : 210.27
SMILES Code : O=C(C1=CC=C(C)C=C1)C2=CC=CC=C2C
MDL No. :MFCD11210909

Safety of [ 1140-16-5 ]

Application In Synthesis of [ 1140-16-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1140-16-5 ]

[ 1140-16-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 615-37-2 ]
  • [ 201230-82-2 ]
  • [ 5720-05-8 ]
  • [ 1140-16-5 ]
YieldReaction ConditionsOperation in experiment
76% With palladium diacetate; sodium carbonate; In water; at 100℃; under 760.051 Torr; for 13h;Sealed tube; Autoclave; Green chemistry; General procedure: A 75 mL autoclave equipped with a Teflon liner and a magnetic stirrer bar was charged with Pd(OAc)2 (4.48 mg, 2.0 × 10-2 mmol), L (46.7 mg, 4.0 × 10-2 mmol) and H2O (6 mL) and the mixture was stirred at room temperatures for 0.5 h under N2. Then iodobenzene (113 μL, 1 mmol), phenylboronic acid (134 mg, 1.1 mmol), Na2CO3(106 mg, 1 mmol), and n-decane (0.1 mL, GC internal standard) were added. Once sealed, the autoclave was purged three times with CO, and pressurized to 1 atm of CO. The reaction mixture was stirred at 100 C for 2 h. After reaction, the mixture was extracted with diethyl ether (3 × 5 mL). The combined organic layer was concentrated in vacuo and the product was purified by column chromatography. In the recycling experiment, the aqueous phase containing the catalyst was subjected to a second run by charging it with the same substrates as mentioned above, and the reaction performed under the same conditions.
 

Historical Records