Alternatived Products of [ 114686-81-6 ]
Product Details of [ 114686-81-6 ]
CAS No. : | 114686-81-6 |
MDL No. : | MFCD08703372 |
Formula : |
C8H6Cl2O
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
189.04
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 114686-81-6 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 114686-81-6 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 114686-81-6 ]
- 1
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[ 114686-85-0 ]
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[ 114686-81-6 ]
Yield | Reaction Conditions | Operation in experiment |
|
With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; water; for 1h; |
A mixture of <strong>[114686-85-0]2-(2,3-dichlorophenyl)ethanol</strong> (0.50 g), NaHCO3 (0.438 g) and Dess-Martin periodinane (1.22 g) in dichloromethane (10 mL) and water (46 mL) was stirred for 1 hour. The mixture was quenched with aqueous NaHCO3 and saturated aqueous Na2S2O3 and extracted with dichloromethane. The extract was dried (Na2SO4), filtered and concentrated. The concentrate was purified on silica gel with an Intelliflash-280 purification system with hexanes/ethyl acetate. |