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[ CAS No. 1150114-73-0 ]

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Chemical Structure| 1150114-73-0
Chemical Structure| 1150114-73-0
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Product Details of [ 1150114-73-0 ]

CAS No. :1150114-73-0 MDL No. :MFCD04112547
Formula : C8H13BClNO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :201.46 g/mol Pubchem ID :44754898
Synonyms :

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Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1150114-73-0 ]

  • Downstream synthetic route of [ 1150114-73-0 ]

[ 1150114-73-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1150114-73-0 ]
  • [ 1379345-12-6 ]
  • [ 2280067-89-0 ]
YieldReaction ConditionsOperation in experiment
75% With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In 1,4-dioxane; water at 80℃; for 6h; Inert atmosphere; 29.2 Step 2. 5-2-4 (700 mg, 2.10 mmol), 4-(dimethylamino)phenylboronic acid hydrochloride (464 mg, 2.31 mmol) and CS2CO3 (2.39 g, 7.34 mmol) were dissolved in 10 mL of 1,4-dioxane and 5 mL of water. Pd(PPh3)4 (121 mg, 0.105 mmol) was added to mixture under inert atmospheric conditions. Reaction mixture was stirred at 80 °C for 6 hours. 250 mL of water was then added, product was extracted with ethyl acetate (3×150 mL). Organic layers were separated, washed with a saturated NaCl solution, and dried with Na2SO4. Product 5-2-3 was isolated as yellow powder by column chromatography on silica gel using hexane-ethyl acetate (9:1) as eluent. Yield: 514 mg (75%).
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