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Chemical Structure| 115022-65-6 Chemical Structure| 115022-65-6

Structure of 115022-65-6

Chemical Structure| 115022-65-6

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Product Details of [ 115022-65-6 ]

CAS No. :115022-65-6
Formula : C12H14O3
M.W : 206.24
SMILES Code : O=C(OC)C1=CC=C(OCCC=C)C=C1

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Application In Synthesis of [ 115022-65-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 115022-65-6 ]

[ 115022-65-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 115022-65-6 ]
  • [ 115595-27-2 ]
YieldReaction ConditionsOperation in experiment
63 g With water; sodium hydroxide; In ethanol; for 4h;Reflux; 76 g of methyl 4-hydroxybenzoate, 54 g of 4-bromo-1-butene and 34 g of potassium carbonate were dissolved in 500 ml of dimethylformamide and stirred at 60 C. for 7 hours.The reaction solution was cooled to room temperature, 1000 ml of water and 100 ml of 10% hydrochloric acid aqueous solution were added,Extraction was performed using toluene, and toluene was distilled off under reduced pressure to obtain 93 g of a crude product of (S-1-1), 108 g.400 ml of water, 400 ml of ethanol and 20 g of sodium hydroxide were added thereto, followed by heating under reflux for 4 hours.After the reaction solution was cooled to room temperature, 500 ml of water was added, and a 10% hydrochloric acid aqueous solution was further added dropwise.The dropwise addition was continued until the aqueous layer became weakly acidic, and crystals precipitated. The precipitated liquid crystal was collected by filtration and dried to obtain 63 g of the compound of (S-1-2).
 

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