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Chemistry
Organic Building Blocks
Bromides
bromophenyl
3-(4-Bromophenyl)-6,9-diphenyl-9H-carbazole
Chemistry
Material Science
Organic Building Blocks
Electronic Materials
Bromides
Benzene Compounds Organic Light-Emitting Diode (OLED) Materials
bromophenyl

[ CAS No. 1186644-47-2 ] {[proInfo.proName]}

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Chemical Structure| 1186644-47-2
Chemical Structure| 1186644-47-2
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Product Details of [ 1186644-47-2 ]

CAS No. :1186644-47-2 MDL No. :
Formula : C30H20BrN Boiling Point : -
Linear Structure Formula :- InChI Key :CMRNTJOPOVHKJQ-UHFFFAOYSA-N
M.W : 474.39 Pubchem ID :58113367
Synonyms :

Safety of [ 1186644-47-2 ]

Signal Word:Warning Class:
Precautionary Statements:P280-P305+P351+P338 UN#:
Hazard Statements:H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1186644-47-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1186644-47-2 ]

[ 1186644-47-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 1622060-65-4 ]
  • [ 1186644-47-2 ]
  • [ 1622060-58-5 ]
YieldReaction ConditionsOperation in experiment
74% With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 24h; Reflux; Inert atmosphere; 4 Synthesis of compound A-93 Example 1 In the synthesized product (G) by the same method as synthesized (H) 10.0 g (21.83 mmol) and intermediate (J) 11.39 g (24.0 mmol) NaO (t-Bu) 3.15 g (32.74 mmol), Pd2(dba)30.40 g (0.44 mmmol) in 150 mL of toluene was suspended after P (t-Bu) 3 0.32 mL (1.31 mmol) into a nitrogen gas stream under stirring under reflux was 24 sigan.Extracted with dichloromethane and distilled water, and the organic layer was purified by silica gel filter.Removing the organic solution hexane: dichloromethane = 7: to give a: 3 (v / v) silica gel column and recrystallized the product solids with dichloromethane and n-hexane A-93 compound 13.8 g (74% yield).
Reference： [1]Current Patent Assignee: SAMSUNG C&T CORPORATION - KR101627750, 2016, B1 Location in patent: Paragraph 0555-0557
  • 2
  • [ 589-87-7 ]
  • [ 1359833-28-5 ]
  • [ 1186644-47-2 ]
YieldReaction ConditionsOperation in experiment
73% With tetrakis(triphenylphosphine) palladium(0); sodium hydroxide In tetrahydrofuran; water Reflux; Synthesis of 3-(4-bromophenyl)-6,9-diphenyl-9H-carbazole After the Sub-1-3 (35.6 g, 80 mmol) obtained in the above synthesis was dissolved in 360 mL THF, 1- bromo-4-iodo-benzene (23.8 g, 84 mmol), Pd(PPh 3 ) 4 (2.8 G, 2.4 mmol), NaOH (9.6 g, 240 mmol) and water (180 mL), and the mixture was refluxed with stirring. After the reaction was completed, the reaction mixture was extracted with ether and water. The organic layer was dried over MgSO 4 and concentrated. The resultingorganic matter was purified and recrystallized from a silica gel column to obtain 27.7 g (73%) of the product.
Reference： [1]Current Patent Assignee: DUK SAN NEOLUX CO., LTD.; DUKSAN HI METAL CO LTD - TWI580673, 2017, B Location in patent: Page/Page column 41; 42
YieldReaction ConditionsOperation in experiment
70% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene for 15h; Heating; Preparation of intermediate 4-(7-bromopyren-2-yl)-N,N-diphenylaniline (B-1) General procedure: 1-1 (183.00g, 450mmol) in 3-neck flask (5L), Bromotriphenylamine (145.89g, 450mmol), tetrakistriphenylphosphine palladium Pd(PPh3) 4 (26g, 22.5mmol) and potassium carbonate (2.2M, 640ml, 1405mmol), toluene (2200ml), ethanol (500 mL) and water (500 mL) were added and heated for 15 hours. The reaction was cooled, filtered and separated, and the toluene layer was dried to obtain a yellow oil. A small amount of dichloromethane was added to dissolve, and an appropriate amount of petroleum ether (PE) was added to obtain a solid B-1 (yield: 153.40 g, 65%). The obtained compound was confirmed by LC-MS.

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Technical Information

• Acid-Catalyzed α -Halogenation of Ketones • Addition of a Hydrogen Halide to an Internal Alkyne • Alcohols from Haloalkanes by Acetate Substitution-Hydrolysis • Alcohols React with PX3 • Alkyl Halide Occurrence • Alkylation of an Alkynyl Anion • An Alkane are Prepared from an Haloalkane • Benzylic Oxidation • Birch Reduction • Birch Reduction of Benzene • Blanc Chloromethylation • Complete Benzylic Oxidations of Alkyl Chains • Complete Benzylic Oxidations of Alkyl Chains • Conversion of Amino with Nitro • Convert Haloalkanes into Alcohols by SN2 • Deprotonation of Methylbenzene • Directing Electron-Donating Effects of Alkyl • Electrophilic Chloromethylation of Polystyrene • Friedel-Crafts Alkylation of Benzene with Acyl Chlorides • Friedel-Crafts Alkylation of Benzene with Carboxylic Anhydrides • Friedel-Crafts Alkylation of Benzene with Haloalkanes • Friedel-Crafts Alkylation Using Alkenes • Friedel-Crafts Alkylations of Benzene Using Alkenes • Friedel-Crafts Alkylations Using Alcohols • Friedel-Crafts Reaction • General Reactivity • Grignard Reaction • Groups that Withdraw Electrons Inductively Are Deactivating and Meta Directing • Halogenation of Alkenes • Halogenation of Benzene • Hiyama Cross-Coupling Reaction • Hydrogenation to Cyclohexane • Hydrogenolysis of Benzyl Ether • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Methylation of Ammonia • Methylation of Ammonia • Nitration of Benzene • Nucleophilic Aromatic Substitution • Nucleophilic Aromatic Substitution with Amine • Oxidation of Alkyl-substituted Benzenes Gives Aromatic Ketones • Preparation of Alkylbenzene • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Dihalides • Reductive Removal of a Diazonium Group • Reverse Sulfonation——Hydrolysis • Stille Coupling • Substitution and Elimination Reactions of Alkyl Halides • Sulfonation of Benzene • Suzuki Coupling • The Acylium Ion Attack Benzene to Form Phenyl Ketones • The Claisen Rearrangement • The Nitro Group Conver to the Amino Function • Vilsmeier-Haack Reaction • Williamson Ether Syntheses
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