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Chemical Structure| 1188094-10-1 Chemical Structure| 1188094-10-1

Structure of 1188094-10-1

Chemical Structure| 1188094-10-1

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Product Details of [ 1188094-10-1 ]

CAS No. :1188094-10-1
Formula : C14H11BO2
M.W : 222.05
SMILES Code : OB(O)C1C=C2C(C3C(C=C2)=CC=CC=3)=CC=1
MDL No. :MFCD16294999

Safety of [ 1188094-10-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 1188094-10-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1188094-10-1 ]

[ 1188094-10-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 121-43-7 ]
  • [ 62162-97-4 ]
  • [ 7732-18-5 ]
  • [ 1188094-10-1 ]
YieldReaction ConditionsOperation in experiment
88% Under nitrogen, 2.57 g (10 mmol) of <strong>[62162-97-4]2-bromophenanthrene</strong> was dissolved in 40 ml of anhydrous THF, the temperature of the reaction was lowered to -78 ° C, After slowly adding 4 ml of 2.5 M n-BuLi dropwise, the reaction was stirred at 0 ° C for 1 hour. Thereafter, the temperature of the reaction was lowered to -78 ° C, 12.47 g (12 mmol) of trimethylborate was added dropwise, and the mixture was stirred at room temperature for 12 hours. After the reaction was completed, 2N-HCl aqueous solution was added, stirred for 30 minutes, and extracted with ether. The water in the organic layer was removed with anhydrous MgSO 4 and the resulting organic layer was concentrated under reduced pressure. The resulting compound was subjected to column chromatography with Hex: MC = 4: 1 to obtain 1.95 g (88percent) of Intermediate-6.
  • 2
  • [ 62162-97-4 ]
  • [ 1188094-10-1 ]
 

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