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Chemical Structure| 1193512-60-5 Chemical Structure| 1193512-60-5

Structure of 1193512-60-5

Chemical Structure| 1193512-60-5

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Product Details of [ 1193512-60-5 ]

CAS No. :1193512-60-5
Formula : C10H19NO2
M.W : 185.26
SMILES Code : O=C([C@H]1CC[C@H](N)CC1)OC(C)C

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Application In Synthesis of [ 1193512-60-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1193512-60-5 ]

[ 1193512-60-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 97-08-5 ]
  • [ 1193512-60-5 ]
  • [ 1357279-63-0 ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20℃; for 4h; Step 1. Preparation of (1r,4r)-isopropyl 4-(4-chloro-3-nitrophenylsulfonamido)cyclohexanecarboxylate; To a solution of (1r,4r)-isopropyl 4-aminocyclohexanecarboxylate (670 mg, 3.44 mmol) in DCM (20 mL) is added 4-chloro-3-nitro-benzenesulfonyl chloride (898 mg, 3.44 mmol) and DIPEA (1.20 mL, 6.87 mmol) at rt. The reaction mixture is stirred for 4 h at rt. The mixture is diluted with DCM and washed with 1 N HCl and saturated aqueous NaCl solution. The organic layer is dried over Na2 SO4, filtered, and concentrated under reduced pressure to yield the title compound as a yellow solid.
 

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