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Chemical Structure| 119511-77-2 Chemical Structure| 119511-77-2

Structure of 119511-77-2

Chemical Structure| 119511-77-2

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Product Details of [ 119511-77-2 ]

CAS No. :119511-77-2
Formula : C12H15NO2
M.W : 205.25
SMILES Code : O=C(C1(N)CCC2=C1C=CC=C2)OCC
MDL No. :MFCD12151764

Safety of [ 119511-77-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 119511-77-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 119511-77-2 ]

[ 119511-77-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 591-68-4 ]
  • [ 119511-77-2 ]
  • [ 407-25-0 ]
  • [ 1292292-81-9 ]
YieldReaction ConditionsOperation in experiment
48% CAL-B (4.5 g, 50 mg/mL) was added to a solution of Compd 2 (0.90 g, 4.39 mmol) and<strong>[591-68-4]BuCO2Bu</strong> (6.34 g, 44.00 mmol) in DIPE (90.0 mL) in the presence of 4 A MS (30 mg/mL). Thereaction was stopped at 49percent conversion by filtering off the enzyme after 24 h. (CF3CO)20 (5.26 g, 21.80 mmol) in CH2C12 (60 mL) was added to the above filtrate and the reaction mixture was stirred for 2 hours before evaporating the solvent. The residue was purified on a silica gel column (petroleum ether/ethyl acetate, 20:1), affording oily N-trifluoroacetylated Compd-3 (Rf = 0.17; 0.69g, 0.70 mmol, 48percent, ee 99percent). LC-MS: m/z = 330.2[M+H]
  • 2
  • [ 591-68-4 ]
  • [ 119511-77-2 ]
  • [ 407-25-0 ]
  • [ 1292292-77-3 ]
  • [ 1292292-81-9 ]
 

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