Home Cart Sign in  
Chemical Structure| 1201221-82-0 Chemical Structure| 1201221-82-0

Structure of 1201221-82-0

Chemical Structure| 1201221-82-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1201221-82-0 ]

CAS No. :1201221-82-0
Formula : C23H37BO6Si
M.W : 448.43
SMILES Code : O=C(C1=CC=C(B2OC(C)(C)C(C)(C)O2)C(C(OC(C)(C)C)=O)=C1)OCC[Si](C)(C)C

Safety of [ 1201221-82-0 ]

Application In Synthesis of [ 1201221-82-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1201221-82-0 ]

[ 1201221-82-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 5985-24-0 ]
  • [ 1201221-82-0 ]
  • 2
  • [ 1201221-82-0 ]
  • [ 57381-62-1 ]
  • 2-(tert-butyl) 2'-methyl 4-(2-(trimethylsilyl)ethyl) 5’-chloro-[1,1‘-biphenyl]-2,2’,4-tricarboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; water; at 65℃; for 12h; Into the reaction vessel containing 1D (2000 mg, 4.46 mmol) was added methyl 2- bromo-4-chlorobenzoate (1335 mg, 5.350 mmol), THF (17 mL), water (17 mL), K2C03 (1849 mg, 13.38 mmol), and Pd(Ph3P)4 (515 mg, 0.446 mmol). The reaction mixture was degassed by bubbling N2 for 10 mm, sealed, and stirred at 65°C for 12h. The reaction mixture was allowed to cool to rt, was concentrated under reduced pressure and subjectedto silica gel chromatography purification to produce hA (1860 mg, 3.79 mmol, 85.0 percent yield). LCMS Anal. Calc?d for C2SH3ICIO6Si 490.16, found {M+Hj 490.8 1HNMR (500MHz, chloroform-d) oe 8.60 (d, J=1.7 Hz, 1H), 8.64 - 8.56 (m, 1H), 8.15 (dd, J=8.0, 1.7 Hz, 1H), 7.99 (d, J8.5 Hz, 1H), 7.43 (dd, J8.5, 2.2 Hz, IH), 7.24 - 7.21 (m, 2H),4.49-4.43 (m, 2H), 3.60 (s, 3H), 1.25 (s, 9H), 1.20- 1.14 (m, 2H), 0.10 (s, 9H).
  • 3
  • [ 1201221-82-0 ]
  • [ 685892-23-3 ]
  • 2-(tert-butyl) 2'-methyl 4-(2-(trimethylsilyl)ethyl) 3'-chloro[1,1'-biphenyl]-2,2',4-tricarboxylate [ No CAS ]
 

Historical Records

Categories