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Chemical Structure| 1204-55-3 Chemical Structure| 1204-55-3

Structure of 1204-55-3

Chemical Structure| 1204-55-3

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Product Details of [ 1204-55-3 ]

CAS No. :1204-55-3
Formula : C10H11NO2S
M.W : 209.26
SMILES Code : CC(SC1=CC=CC=C1NC(C)=O)=O

Safety of [ 1204-55-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P264-P270-P301+P312-P330-P501

Application In Synthesis of [ 1204-55-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1204-55-3 ]

[ 1204-55-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2401-21-0 ]
  • [ 1204-55-3 ]
  • [ 1910-85-6 ]
YieldReaction ConditionsOperation in experiment
64% With caesium carbonate; In N,N-dimethyl-formamide; at 130℃; for 10h;Inert atmosphere; General procedure: To an oven-dried 25 mL ground mouth test tube equipped with a stir bar was added S-2-acetamidophenyl ethanethioate (0.5 mmol), 1-bromo-2-iodobenzene (0.6 mmol), Cs2CO3 (2.0 mmol), DMF (3 mL). The test tube was sealed with a sleeve rubber stopper and evacuated and refilled with argon for three cycles. The mixture was stirred 130 oC for 10 hours. After cooling to room temperature, the reaction mixture was quenched with water (20 mL), and extracted with ethyl acetate (20 mL) for three times. The combined organic layer was dried with anhydrous MgSO4, and condensed in vacuum on a rotary evaporator. The residual was purified on a silica gel chromatograph column by means of gradient elution (eluent: petroleum ether / ethyl acetate) to give the desired product. #10;
 

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