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Chemical Structure| 120758-24-9 Chemical Structure| 120758-24-9

Structure of 120758-24-9

Chemical Structure| 120758-24-9

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Product Details of [ 120758-24-9 ]

CAS No. :120758-24-9
Formula : C17H20O4S
M.W : 320.40
SMILES Code : O=S(C1=CC=C(C)C=C1)(OCCCOCC2=CC=CC=C2)=O
MDL No. :MFCD28405989

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Application In Synthesis of [ 120758-24-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 120758-24-9 ]

[ 120758-24-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 101-06-4 ]
  • [ 120758-24-9 ]
  • [ 1325724-17-1 ]
YieldReaction ConditionsOperation in experiment
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In water; toluene; at 50 - 80℃; for 19h; To a solution of alcohol and tosylate in toluene would be added a 50% aqueous NaOH solution and tetrabutylammonium hydrogen sulfate. The reaction mixture would be stirred at 80 C. for 3 h then stirred at 50 C. for 16 h. After completion of the reaction, an aqueous ammonium chloride solution would be added, and the reaction mixture would be further diluted with ethyl acetate. The phases would be separated, and the aqueous phase would be extracted with ethyl acetate. The combined organic phases would be dried over anhydrous sodium sulfate, filtered, and concentrated in vacuo.; Dibenzyl-[2-(3-benzyloxy-propoxy)-ethyl]-amine (860 mg) was prepared by following General Procedure W starting from toluene-4-sulfonic acid 3-benzyloxy-propyl ester (1.33 g), <strong>[101-06-4]N,N-dibenzyl-2-aminoethanol</strong> (1.0 g), 50% aqueous sodium hydroxide solution (1.66 g in 1.66 mL of water), and tetrabutylammonium hydrogen sulfate (141 mg).
 

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