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Chemical Structure| 1208075-03-9 Chemical Structure| 1208075-03-9

Structure of 1208075-03-9

Chemical Structure| 1208075-03-9

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Product Details of [ 1208075-03-9 ]

CAS No. :1208075-03-9
Formula : C7H5FN2O3
M.W : 184.13
SMILES Code : O=C(N)C1=CC([N+]([O-])=O)=CC(F)=C1
MDL No. :MFCD08447279

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1208075-03-9 ]

[ 1208075-03-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110882-60-5 ]
  • [ 1208075-03-9 ]
YieldReaction ConditionsOperation in experiment
36% With sulfuric acid; water; trifluoroacetic acid; at 70℃; for 24.0h; Step 1To a solution of <strong>[110882-60-5]3-fluoro-5-nitrobenzonitrile</strong> (1.0 g, 6.02 mmoL) in TFA (8 mL) was added water (1 mL) and cone, sulfuric acid (2 mL). The reaction mixture was heated to 70 °C and stirred for 24 h. Then the reaction mixture was cooled to 0 °C and liquid ammonia solution was added. The solidified solid was filtered through Celite.(R). (diatomaceous earth) and washed with water to obtain 3-fluoro-5-nitrobenzamide (0.400 g, 36percent>) as an off white solid. Observed mass (M-l): 183.02.
 

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