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[ CAS No. 1215767-84-2 ] {[proInfo.proName]}

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Chemical Structure| 1215767-84-2
Chemical Structure| 1215767-84-2
Structure of 1215767-84-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1215767-84-2 ]

CAS No. :1215767-84-2 MDL No. :MFCD22628043
Formula : C9H5BrClN Boiling Point : -
Linear Structure Formula :- InChI Key :CMWLIWRAKZQZII-UHFFFAOYSA-N
M.W : 242.50 Pubchem ID :58349436
Synonyms :

Safety of [ 1215767-84-2 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1215767-84-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1215767-84-2 ]

[ 1215767-84-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 96558-78-0 ]
  • [ 56-81-5 ]
  • [ 1215767-84-2 ]
  • 7-bromo-5-chloroquinoline [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid; nitrobenzene; at 150℃; for 3h;Inert atmosphere; <strong>[96558-78-0]3-chloro-5-bromoaniline</strong> (1 g, 4.84 mmol) was dissolv ed in 75% I LSO ( 10 mL). Then glycerol (1.1 1 g, 12.1 mmol ) and nitrobenzene (0.59 g. 4.84 mmol ) were added. The reaction mixture was stirred at 150C for 3 hours under N2. EtOAc (50 ml ) was added and the mixture was adjusted to pH to 6-7 with a 30% solution of NaOH in water. The solid was filtered off over celite and the organic layer was separated and ev aporated. The residue was purified by flash column chromatograph over silica gel (gradient eiuent: petroleum ether EtOAc from 20/ 1 to 5/1). The desired fractions were collected and the solvent was evaporated to give a mixture of intermediate 457 and intermediate 458 (750 mg) as a white solid.
  • 2
  • [ 53472-18-7 ]
  • [ 1215767-84-2 ]
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