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CAS No. : | 121821-01-0 | MDL No. : | MFCD00035196 |
Formula : | C11H13ClN2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GEFZFHTWRMQGOO-UHFFFAOYSA-N |
M.W : | 240.69 | Pubchem ID : | 14374493 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With triethylamine In toluene at 70℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
98% | With pyridine; triethylamine for 4h; Ambient temperature; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
98% | With hydrogenchloride In ethanol at 75℃; for 5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
85% | With triethylamine In tetrahydrofuran Ambient temperature; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: N2H4*H2O / ethanol; dimethylformamide 2: 98 percent / 2M HCl / ethanol / 5 h / 75 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C 4: 95 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature | ||
Multi-step reaction with 2 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: 95 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C 4: 99 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C 4: 88 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C 4: 98 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 98 percent / Et3N, pyridine / 4 h / Ambient temperature 2: NaNO2 / acetic acid; acetic anhydride / 3 h / 5 °C 3: benzene / 20 h / 80 °C 4: 99 percent / Cs2CO3 / dimethylformamide / 48 h / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
11% | With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 23℃; for 3h; | C To a solution of 2-(3-aminopropyl)isoindoline-l,3-dione hydrochloride (49.8 mg, 0.207 mmol), malonic acid (43.1 mg, 2.0 equiv.), and DIPEA (0.11 mL, 3.0 equiv.) in DMF (0.9 mL) was added HATU (157.3 mg, 2.0 equiv.). The reaction mixture was agitated at ambient temperature for 3 hours and then purified by preparative HPLC (H20/MeCN with 0.1% TFA) to afford 6.7 mg (11% yield) of 1-94 as a colorless oil. ESI-MS: Found 291.1, C14H15N2O5 (MH+) requires 291.1 |
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