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Chemical Structure| 1221274-40-3 Chemical Structure| 1221274-40-3

Structure of 1221274-40-3

Chemical Structure| 1221274-40-3

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Product Details of [ 1221274-40-3 ]

CAS No. :1221274-40-3
Formula : C19H21NO3
M.W : 311.38
SMILES Code : O=C(OCC1C2=C(C3=C1C=CC=C3)C=CC=C2)N[C@@H](C)CCO
MDL No. :N/A

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Application In Synthesis of [ 1221274-40-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1221274-40-3 ]

[ 1221274-40-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 193954-26-6 ]
  • [ 1221274-40-3 ]
YieldReaction ConditionsOperation in experiment
96% General procedure: To a solution of carboxylic acid (10 mmol) in THF (10 mL), DIPEA (11 mmol, 1.42 mL) and 50% T3P in EtOAc (20 mmol, 6.36 mL) were added at 0 C and the solution was stirred for about 10 min. Then aqueous solution of NaBH4 (10 mmol, 388 mg in 0.3 mL of H2O) was added to the reaction mixture at the same temperature and the reaction was allowed to stir till the completion of the reaction as indicated by TLC. After the completion of the reaction, the solvent was evaporated and the crude alcohol was extracted into EtOAc and the organic phase was washed with 5% citric acid (10 mL × 2), 5% Na2CO3 (10 mL × 2), water, and brine solution. The product was isolated after the evaporation of solvent under reduced pressure and dried over anhydrous Na2SO4.
 

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