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CAS No. : | 1228880-71-4 | MDL No. : | |
Formula : | C8H10N2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 150.18 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With hydrogen;palladium on activated charcoal; In ethanol; at 20℃; under 2585.81 Torr; for 12h;Product distribution / selectivity; | Step 6: Preparation of 5,6-diamino-2,3-dihydrobenzofuran [Show Image] The product obtained in Step 5 (2.5 g, 13.9 mmol) and Pd/C(0.5 g) were dissolved in EtOH (50 mL), hydrogenated in a Parr hydrogenation apparatus at room temperature and a hydrogen pressure of 50 PSI for 12 h. The catalyst was removed by filtration, the ethanol solution of the product was directly used in the next step of reaction. |