Home Cart Sign in  
Chemical Structure| 1233494-98-8 Chemical Structure| 1233494-98-8

Structure of H-D-Ser(Bzl)-OH·HCl
CAS No.: 1233494-98-8

Chemical Structure| 1233494-98-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1233494-98-8 ]

CAS No. :1233494-98-8
Formula : C10H14ClNO3
M.W : 231.68
SMILES Code : O=C(O)[C@H](N)COCC1=CC=CC=C1.[H]Cl
MDL No. :MFCD04112475
InChI Key :FUJXTCPYWRWTDZ-SBSPUUFOSA-N
Pubchem ID :53229898

Safety of [ 1233494-98-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1233494-98-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1233494-98-8 ]

[ 1233494-98-8 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 84907-81-3 ]
  • [ 1233494-98-8 ]
  • 2
  • [ 1233494-98-8 ]
  • [ 10433-52-0 ]
  • 3
  • [ 3587-60-8 ]
  • [ 1233494-98-8 ]
  • 4
  • [ 84907-79-9 ]
  • [ 1233494-98-8 ]
  • 5
  • [ 84907-80-2 ]
  • [ 1233494-98-8 ]
  • 6
  • [ 1233494-98-8 ]
  • [ 75-07-0 ]
  • [ 76-05-1 ]
  • [ 1007880-70-7 ]
YieldReaction ConditionsOperation in experiment
NaBH3CN (1.6 g, 25.5 mmol) was added to a cooled (ice/water bath) water(25 ml)/methanol (15 ml) solution of <strong>[1233494-98-8]H-D-Ser-OBzl HCl</strong> (2.0 g, 8.6 mmol). Acetaldehyde (1.5 ml, 12.5 mmol) was added drop-wise over 5 min, the cooling bath was removed, and the reaction mixture was stirred at ambient condition for 2 hr. The reaction was carefully quenched with 12N HCl and concentrated in vacuo. The residue was dissolved in water and purified with a reverse phase HPLC(MeOH/H2O/TFA) to afford the TFA salt of (R)-benzyl 2-(diethylamino)-3- hydroxypropanoate as a colorless viscous oil (1.9g). 1H NMR (DMSO-dβ, δ = 2.5 ppm, 500 MHz): δ 9.73 (br s, IH), 7.52-7.36 (m, 5H), 5.32 (d, J = 12.2, IH), 5.27 (d, J = 12.5, IH), 4.54-4.32 (m, IH), 4.05-3.97 (m, 2H), 3.43-3.21 (m, 4H), 1.23 (t, J = 7.2, 6H). LC/MS (Cond. 2): RT = 1.38 min; LC/MS: Anal. Calcd. for [M+H]+ Ci4H22NO3: 252.16; found 252.19.
  • 7
  • [ 1233494-98-8 ]
  • [ 75-07-0 ]
  • [ 76-05-1 ]
  • (R)-benzyl 2-(diethylamino)-3-hydroxypropanoate trifluroacetate [ No CAS ]
YieldReaction ConditionsOperation in experiment
NaBH3CN (1.6 g, 25.5 mmol) was added to a cooled (ice/water bath) water(25 ml)/methanol (15 ml) solution of <strong>[1233494-98-8]H-D-Ser-OBzl HCl</strong> (2.0 g, 8.6 mmol). Acetaldehyde (1.5 ml, 12.5 mmol) was added drop-wise over 5 min, the cooling bath was removed, and the reaction mixture was stirred at ambient condition for 2 hr. The reaction was carefully quenched with 12N HCl and concentrated in vacuo. The residue was dissolved in water and purified with a reverse phase HPLC (MeOH/H2O/TFA) to afford the TFA salt of (R)-benzyl 2-(diethylamino)-3- hydroxypropanoate as a colorless viscous oil (1.9g), 1H NMR (DMSO-dg, 5 = 2.5 ppm, 500 MHz): δ 9.73 (br s, IH), 7.52-7.36 (m, 5H), 5.32 (d, J - 12.2, IH), 5.27 (d, J - 12.5, IH), 4.54-4.32 (m, IH), 4.05-3.97 (m, 2H), 3.43-3.21 (m, 4H), 1.23 (t, J = 7.2, 6H). LC/MS (Cond. 2): RT = 1.38 min; LC/MS: Anal. Calcd. for [M+H]+ C] 4H22NO3: 252.16; found 252.19.
  • 8
  • [ 1233494-98-8 ]
  • H-D-Ser-OBzl*HCl [ No CAS ]
 

Historical Records