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CAS No. : | 1240327-15-4 | MDL No. : | N/A |
Formula : | C14H11NO5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | ANYWVTSQEOSVIU-UHFFFAOYSA-N |
M.W : | 273.24 | Pubchem ID : | 102046936 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 | UN#: | N/A |
Hazard Statements: | H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
45% | With melamine In ethanol; water High Pressure; mixt. of Pb(CH3COO)2*3H2O, 5-(pyridin-4-ylmethoxy)-isophthalic acid and melamine dissolved in EtOH/H2O; soln. sealed in Teflon-lined autoclave at 160°C for 60 h and then slowly cooled to room temp.; elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
65% | With sodium hydroxide In water at 100℃; for 72h; Autoclave; | General procedure for the preparation of complex 1. A mixture of Mn(NO3)2·6H2O (29.7 mg, 0.1 mmol) and H2L12 (17.2 mg, 0.1 mmol)was added to 8 ml of DMF/H2O (1:3, v/v) and adjusted to pH 6.0-7.0 with 1 M NaOH. The final mixture was placed in a Parr Teflon-lined stainless steel vessel (15 ml) under autogenous pressure and heated at 100 °C for three days; colorless crystals were obtained (yield 65% based on Mn). IR (KBr, n/cm-1): 3437 (s), 1657 (s), 1617 (m), 1584 (m), 1548(s), 1448 (m), 1413 (m), 1377 (s), 1277 (w), 1246 (w), 1127 (w), 1102 (w), 1052 (m), 924 (w), 784 (m), 720 (m), 668 (m), 633 (w), 572 (w), 482 (w), 421 (w). Found (%): C, 48.12; H, 4.67; N, 6.52. Calc. for C34H36Mn2N4O14(%): C, 48.93; H, 4.35; N, 6.71. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
65% | In water at 160℃; for 60h; Autoclave; High pressure; | Synthesis of [Dy4(L)6(H2O)4]n (1) Synthesis of [Dy4(L)6(H2O)4]n (1). A mixture of Dy(NO3)26H2O (0.5 mmol), H2L (0.2 mmol), and 12 mLH2O was placed in a Parr Teflon-lined stainless steel vessel (25 mL), and then the vessel was sealed and heated to160C. The temperature was hold for 60 h, then the vesselwas cooled to room temperature over 60 h. Orangecrystals of 1were obtained with the yields of 65% basedon the H2L ligand. Elemental Anal. Calcd. (%)C84H62N6O34Dy4: C, 42.91; H, 2.64; N, 3.58%. Found: C,42.88; H, 2.67, N, 3.54%. IR (solid KBr pellet,v/cm1)for 1: 3127(m), 2891(m), 1642(s), 1612(s), 1561(s), 1448(s),1367(m), 1258(m), 1131(m), 1062(w); 852(vw), 775(w), 711(vw), 612(w). |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70.3% | Stage #1: 4,4'-bipyridine; cadmium(II) nitrate tetrhydrate; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
67.9% | Stage #1: cadmium(II) nitrate tetrhydrate; terephthalic acid; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
60.5% | Stage #1: cadmium(II) nitrate tetrhydrate; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
91.7% | With hydrogenchloride In ethanol; acetonitrile at 119.84℃; for 72h; Autoclave; High pressure; |