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[ CAS No. 1240327-15-4 ] {[proInfo.proName]}

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Chemical Structure| 1240327-15-4
Chemical Structure| 1240327-15-4
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Product Details of [ 1240327-15-4 ]

CAS No. :1240327-15-4 MDL No. :N/A
Formula : C14H11NO5 Boiling Point : -
Linear Structure Formula :- InChI Key :ANYWVTSQEOSVIU-UHFFFAOYSA-N
M.W : 273.24 Pubchem ID :102046936
Synonyms :

Safety of [ 1240327-15-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1240327-15-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1240327-15-4 ]

[ 1240327-15-4 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 1240327-15-4 ]
  • [ 6080-56-4 ]
  • [Pb2(5-(pyridin-4-ylmethoxy)-isophthalate)2] [ No CAS ]
YieldReaction ConditionsOperation in experiment
45% With melamine In ethanol; water High Pressure; mixt. of Pb(CH3COO)2*3H2O, 5-(pyridin-4-ylmethoxy)-isophthalic acid and melamine dissolved in EtOH/H2O; soln. sealed in Teflon-lined autoclave at 160°C for 60 h and then slowly cooled to room temp.; elem. anal.;
  • 2
  • manganese(II) nitrate hexahydrate [ No CAS ]
  • [ 1240327-15-4 ]
  • [ 33513-42-7 ]
  • 2C14H9NO5(2-)*4H2O*2C3H7NO*2Mn(2+) [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% With sodium hydroxide In water at 100℃; for 72h; Autoclave; General procedure for the preparation of complex 1. A mixture of Mn(NO3)2·6H2O (29.7 mg, 0.1 mmol) and H2L12 (17.2 mg, 0.1 mmol)was added to 8 ml of DMF/H2O (1:3, v/v) and adjusted to pH 6.0-7.0 with 1 M NaOH. The final mixture was placed in a Parr Teflon-lined stainless steel vessel (15 ml) under autogenous pressure and heated at 100 °C for three days; colorless crystals were obtained (yield 65% based on Mn). IR (KBr, n/cm-1): 3437 (s), 1657 (s), 1617 (m), 1584 (m), 1548(s), 1448 (m), 1413 (m), 1377 (s), 1277 (w), 1246 (w), 1127 (w), 1102 (w), 1052 (m), 924 (w), 784 (m), 720 (m), 668 (m), 633 (w), 572 (w), 482 (w), 421 (w). Found (%): C, 48.12; H, 4.67; N, 6.52. Calc. for C34H36Mn2N4O14(%): C, 48.93; H, 4.35; N, 6.71.
  • 3
  • dysprosium(III) nitrate hexahydrate [ No CAS ]
  • [ 1240327-15-4 ]
  • 4Dy(3+)*6C14H9NO5(2-)*4H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% In water at 160℃; for 60h; Autoclave; High pressure; Synthesis of [Dy4(L)6(H2O)4]n (1) Synthesis of [Dy4(L)6(H2O)4]n (1). A mixture of Dy(NO3)26H2O (0.5 mmol), H2L (0.2 mmol), and 12 mLH2O was placed in a Parr Teflon-lined stainless steel vessel (25 mL), and then the vessel was sealed and heated to160C. The temperature was hold for 60 h, then the vesselwas cooled to room temperature over 60 h. Orangecrystals of 1were obtained with the yields of 65% basedon the H2L ligand. Elemental Anal. Calcd. (%)C84H62N6O34Dy4: C, 42.91; H, 2.64; N, 3.58%. Found: C,42.88; H, 2.67, N, 3.54%. IR (solid KBr pellet,v/cm1)for 1: 3127(m), 2891(m), 1642(s), 1612(s), 1561(s), 1448(s),1367(m), 1258(m), 1131(m), 1062(w); 852(vw), 775(w), 711(vw), 612(w).
  • 4
  • [ 553-26-4 ]
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 1240327-15-4 ]
  • [ 7732-18-5 ]
  • C14H9NO5(2-)*Cd(2+)*2H2O*0.5C10H8N2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
70.3% Stage #1: 4,4'-bipyridine; cadmium(II) nitrate tetrhydrate; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation;
  • 5
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 100-21-0 ]
  • [ 1240327-15-4 ]
  • [ 7732-18-5 ]
  • 0.5C8H6O4*C14H9NO5(2-)*Cd(2+)*2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
67.9% Stage #1: cadmium(II) nitrate tetrhydrate; terephthalic acid; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation;
  • 6
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 1240327-15-4 ]
  • [ 7732-18-5 ]
  • C14H9NO5(2-)*Cd(2+)*3H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
60.5% Stage #1: cadmium(II) nitrate tetrhydrate; 5-(pyridin-4-ylmethoxy)-isophthalic acid; water With nitric acid In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: In N,N-dimethyl-formamide for 0.05h; Microwave irradiation;
  • 7
  • indium(III) chloride [ No CAS ]
  • [ 1240327-15-4 ]
  • [ 7732-18-5 ]
  • C14H9NO5(2-)*In(3+)*Cl(1-)*2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
91.7% With hydrogenchloride In ethanol; acetonitrile at 119.84℃; for 72h; Autoclave; High pressure;
  • 8
  • [ 1240327-15-4 ]
  • [ 7732-18-5 ]
  • HIn(2+)*2NO3(1-)*4H2O [ No CAS ]
  • C14H9NO5(2-)*In(3+)*H2O*NO3(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
93.1% With nitric acid In acetonitrile at 99.84℃; for 72h; Autoclave; High pressure;
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