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Chemical Structure| 1251503-35-1 Chemical Structure| 1251503-35-1

Structure of 1251503-35-1

Chemical Structure| 1251503-35-1

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Product Details of [ 1251503-35-1 ]

CAS No. :1251503-35-1
Formula : C22H15N3
M.W : 321.38
SMILES Code : C1(NC2=C3N=CC=C2)=C3C=C(C4=C(C5=NC=CC=C5)C=CC=C4)C=C1
MDL No. :MFCD29089368

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Application In Synthesis of [ 1251503-35-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1251503-35-1 ]

[ 1251503-35-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 10016-52-1 ]
  • [ 1251503-35-1 ]
  • [ 1196704-81-0 ]
YieldReaction ConditionsOperation in experiment
71% Under a stream of nitrogen, 0.46 g (1.4 mmol) of <strong>[10016-52-1]2,8-dibromodibenzofuran</strong> (manufactured by Sigma-Aldrich Co. LLC.) and 0.90 g (2.8 mmol) of Exemplified Compound 18-1 were added to 15 ml of DMSO and 0.89 g (4.2 mmol) of potassium phosphate and stirred for 10 minutes. To the resultant, 53 mg (0.28 mmol) of CuI and 6-methyl picolinic acid (0.56 mmol) were added and heated at 125° C. for 7 hours. Under cooling with water, 5 ml of water was added thereto and stirred for 1 hour. The precipitated crude product was filtered, further subjected to the column purification, and then recrystallized with o-dichlorobenzene/acetonitrile so as to obtain 0.80 g (yield of 71percent) of Exemplified Compound 18.
 

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