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Chemical Structure| 1255207-13-6 Chemical Structure| 1255207-13-6

Structure of 1255207-13-6

Chemical Structure| 1255207-13-6

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Product Details of [ 1255207-13-6 ]

CAS No. :1255207-13-6
Formula : C11H10O3
M.W : 190.20
SMILES Code : O=CCC1=C(C2=C(C=C1)C(OC2)=O)C
MDL No. :MFCD24687159

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Application In Synthesis of [ 1255207-13-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1255207-13-6 ]

[ 1255207-13-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1255207-13-6 ]
  • [ 138007-24-6 ]
  • tert-butyl 1-(2-(4-methyl-1-oxo-1,3-dihydroisobenzofuran-5-yl)ethyl)piperidine-4-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
A solution of 2-(4-methyl- 1 -oxo- 1,3 -dihydroisobenzofuran-5 -yl)acetaldehyde (3.20g, 16.8 mmol), <strong>[138007-24-6]ter<strong>[138007-24-6]t-butyl piperidine-4-carboxylate</strong></strong> (3.10 g, 16.8 mmol) and AcOH (2 drops) in MeOH (15 mL)was stirred at 70 OC for 1 hour. Then NaCNBH3 (3.10 g, 50.4 mmol) was added. The reaction mixture was stirred at 70 OC overnight. After cooling to r.t., the mixture was concentrated in vacuo. The mixture was filtered and purified by column chromatography to afford the title product.
 

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