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Chemical Structure| 126084-11-5 Chemical Structure| 126084-11-5

Structure of 126084-11-5

Chemical Structure| 126084-11-5

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Product Details of [ 126084-11-5 ]

CAS No. :126084-11-5
Formula : C9H11NO3
M.W : 181.19
SMILES Code : O=C(C1=CC=C(C)N=C1OC)OC
MDL No. :MFCD16611639

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Application In Synthesis of [ 126084-11-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 126084-11-5 ]

[ 126084-11-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 38116-61-9 ]
  • [ 74-88-4 ]
  • [ 126084-11-5 ]
YieldReaction ConditionsOperation in experiment
With silver carbonate; In chloroform; at 65℃; for 16h;Inert atmosphere;Product distribution / selectivity; To a stirred mixture of <strong>[38116-61-9]2-hydroxy-6-methylnicotinic acid</strong> (5.00 g, 32.7 mmol) in chloroform (160 mL) under an atmosphere of nitrogen was added silver carbonate (9.00 g, 32.7 mmol) and methyl iodide (6.11 mL, 98.0 mmol). The reaction mixture was heated at 65 C for 16 hours. The mixture was allowed to cool and filtered through Celite and the filtrate was concentrated under reduced pressure to give methyl 2-methoxy-6-methylnicotinate (5.60 g) which was used without purification.
 

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