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CAS No. : | 1261475-45-9 | MDL No. : | MFCD18392284 |
Formula : | C7H6BrNO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CGVQNXRJFYFTDX-UHFFFAOYSA-N |
M.W : | 232.03 | Pubchem ID : | 72207207 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H317-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
67.7% | With manganese(IV) oxide In 1,2-dichloro-ethaneReflux | 14.0 g of 3-bromo-2-nitrobenzyl alcohol and 150 mL of 1,2-dichloroethane were placed in a three-necked flask, and 42.0 g of manganese dioxide was added thereto, followed by heating to reflux. After the reaction was completed, it was added to Celite, and the filtrate was concentrated.Column was isolated to give 9.4 g (67.7percent) of 3-bromo-2-nitrobenzaldehyde. |
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