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CAS No. : | 1263413-38-2 | MDL No. : | |
Formula : | C7H7IN2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 278.05 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In methanol; at 20℃; | 1-Fluoro-3-iodo-2-nitrobenzene (2.67 g, 10 mmol; Apollo) and methylamine (2.87 g, 27% w/w solution in MeOH) were dissolved in MeOH (50 ml.) and stirred at RT overnight. The mixture was concentrated to afford the title compound (2.22 g) as a red solid. |