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Chemical Structure| 1269004-46-7 Chemical Structure| 1269004-46-7

Structure of 1269004-46-7

Chemical Structure| 1269004-46-7

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Product Details of [ 1269004-46-7 ]

CAS No. :1269004-46-7
Formula : C42H62B2N2O6S2
M.W : 776.71
SMILES Code : O=C1N(CC(CC)CCCC)C(C2=CC=C(B3OC(C)(C)C(C)(C)O3)S2)=C4C1=C(C5=CC=C(B6OC(C)(C)C(C)(C)O6)S5)N(CC(CC)CCCC)C4=O
InChI Key :DMWRDBVIELOJDX-UHFFFAOYSA-N
Pubchem ID :53242291

Safety of [ 1269004-46-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1269004-46-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1269004-46-7 ]

[ 1269004-46-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1000623-95-9 ]
  • [ 73183-34-3 ]
  • [ 1269004-46-7 ]
YieldReaction ConditionsOperation in experiment
53.4% With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; In 1,4-dioxane; at 120℃; for 15h;Inert atmosphere; After making the gas in the 100 mL flask under a nitrogen gas air current atmosphere,Compound 13 (manufactured by Luminescence Technology, 3.70 g, 5.4 mmoll), bis (pinacolato) diboron(3.00 g, 11.8 mmol), potassium acetate(2.59 g, 26.4 mmol),[1,1'-bis (diphenylphosphino) ferrocene] palladium (II)Dichloride dichloromethane adduct (0.09 g, 0.1 mmol),1,1'-bis (diphenylphosphino) ferrocene(0.06 g, 0.1 mmol) and anhydrous 1,4-dioxane (300 mL)At room temperature, and the mixture was heated under stirring at 120 C. for 15 hours.The obtained reaction solution was filtered through Celite, and the obtained Celite was dissolved in chloroform(200 mL) for 5 times.The obtained filtrate was concentrated by an evaporator, and to the obtained residue was added chloroform(200 mL), and the mixture was heated and stirred at 80 C., then acetonitrile(400 mL) was added, and the mixture was allowed to cool to room temperature while stirring,The mixture was further stirred at room temperature for 1 hour. The obtained solid was collected by filtration,After washing twice with acetonitrile (100 mL)And dried under reduced pressure to obtain Compound 14.The yield of compound 14 was 2.25 g (0.24 mmol), and the yield was 53.4%.
 

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