Home Cart Sign in  
Chemical Structure| 126993-72-4 Chemical Structure| 126993-72-4

Structure of 126993-72-4

Chemical Structure| 126993-72-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 126993-72-4 ]

CAS No. :126993-72-4
Formula : C11H11N3O
M.W : 201.22
SMILES Code : NC1=NC(OCC2=CC=CC=C2)=CN=C1

Safety of [ 126993-72-4 ]

Application In Synthesis of [ 126993-72-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 126993-72-4 ]

[ 126993-72-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 33332-28-4 ]
  • [ 100-51-6 ]
  • [ 126993-72-4 ]
YieldReaction ConditionsOperation in experiment
19% General procedure: [0275] To anhydrous DMF was added sodium hydride (1.2 equiv., 60 % dispersion) and allowed to stir for 1 min. To this stirred mixture was added portion wise a solution of benzyl alcohol (1.2 equiv.) in anhydrous DMF (0.1 M). The mixture was stirred at room temperature for 30 min and then a solution of 6-chloropyrazin-2-amine in anhydrous DMF (0.1 M) was added. The reaction was allowed to stir at 100 C for 16 h and upon completion was quenched slowly with isopropanol. The reaction was then partitioned between ethyl acetate and water. The organic layer was washed with water 3X, brine 3X, and then dried over sodium sulfate. The combined organic layers were concentrated under reduced pressure and the product purified via silica gel chromatography.
 

Historical Records