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Chemical Structure| 127234-68-8 Chemical Structure| 127234-68-8

Structure of 127234-68-8

Chemical Structure| 127234-68-8

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Product Details of [ 127234-68-8 ]

CAS No. :127234-68-8
Formula : C20H19NO2
M.W : 305.38
SMILES Code : O=C1C(OCC2=CC=CC=C2)=C(C)N(CC3=CC=CC=C3)C=C1
MDL No. :MFCD00215669

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Application In Synthesis of [ 127234-68-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 127234-68-8 ]

[ 127234-68-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 61160-18-7 ]
  • [ 100-39-0 ]
  • [ 584-08-7 ]
  • [ 127234-68-8 ]
YieldReaction ConditionsOperation in experiment
70% In ethanol; Petroleum ether; EXAMPLE 3a 1-(phenylmethyl)-2-methyl-3-(phenylmethoxy) 4-pyridone 73 g of the product of Example 2 were dissolved in 4 liters of ethanol (dry). 25 g K2 CO3 powderized and 70 g benzylbromide were added. After refluxing for 4 hours and filtration, the solvent was distilled off and the residue extracted with 4 liters of hot petroleum ether in 3 parts. After cooling to room temperature and filtration the petroleum ether filtrate was concentrated to 2 liters and cooled to -10° C. 31 g of white crystals of the title compound of Example 3 were obtained. The formed title compound 3A was insoluble in petroleum ether at room temperature white crystals. 70percent of total yield.
  • 2
  • [ 61160-18-7 ]
  • [ 100-44-7 ]
  • [ 127234-68-8 ]
 

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