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CAS No. : | 127682-66-0 | MDL No. : | MFCD17170619 |
Formula : | C8H8N2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 164.16 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
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In sodium hydroxide; ethanol | 66 6-Amino-2-pyridinemethanamine Preparation 66 6-Amino-2-pyridinemethanamine A solution of 6-acetylaminopyridine-2-carboxaldehyde1 (0.65 g, 3.96 mmole) in ethanol (150 ml) was saturated with ammonia and hydrogenated over 10% Pd--C (0.32 g) for 24 h. The catalyst was removed by filtration through kieselguhr and the catalyst was washed with ethanol (2*50 ml). The filtrate and wash were evaporated to leave a solid which was taken up in 2M sodium hydroxide solution (20 ml) and heated at 60° for 2 h. The cooled mixture was evaporated to low bulk (~1.5 ml) and extracted with dichloromethane (5*20 ml). The extract was dried (MgSO4) and evaporated to leave the crude title compound as an oil which was used without further purification. |