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[ CAS No. 127682-66-0 ] {[proInfo.proName]}

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Chemical Structure| 127682-66-0
Chemical Structure| 127682-66-0
Structure of 127682-66-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 127682-66-0 ]

CAS No. :127682-66-0 MDL No. :MFCD17170619
Formula : C8H8N2O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 164.16 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 127682-66-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 127682-66-0 ]

[ 127682-66-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 127682-66-0 ]
  • [ 167298-54-6 ]
YieldReaction ConditionsOperation in experiment
In sodium hydroxide; ethanol 66 6-Amino-2-pyridinemethanamine Preparation 66 6-Amino-2-pyridinemethanamine A solution of 6-acetylaminopyridine-2-carboxaldehyde1 (0.65 g, 3.96 mmole) in ethanol (150 ml) was saturated with ammonia and hydrogenated over 10% Pd--C (0.32 g) for 24 h. The catalyst was removed by filtration through kieselguhr and the catalyst was washed with ethanol (2*50 ml). The filtrate and wash were evaporated to leave a solid which was taken up in 2M sodium hydroxide solution (20 ml) and heated at 60° for 2 h. The cooled mixture was evaporated to low bulk (~1.5 ml) and extracted with dichloromethane (5*20 ml). The extract was dried (MgSO4) and evaporated to leave the crude title compound as an oil which was used without further purification.
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