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Chemical Structure| 128094-16-6 Chemical Structure| 128094-16-6

Structure of 128094-16-6

Chemical Structure| 128094-16-6

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Product Details of [ 128094-16-6 ]

CAS No. :128094-16-6
Formula : C10H9BrN2
M.W : 237.10
SMILES Code : NC1=C2C(N)=CC=CC2=C(Br)C=C1

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Application In Synthesis of [ 128094-16-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 128094-16-6 ]

[ 128094-16-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 654664-63-8 ]
  • [ 128094-16-6 ]
  • C28H20N2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
87% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; for 4h;Reflux; Inert atmosphere; In a 500mL three-neck flask under nitrogen protection, 4 bromo-1,8-dinaphthylamine (11.8 g, 0.05 mol) was added, 2-triphenyleneboronic acid (13.6 g, 0.05 mol), a mixture of tetrakistriphenylphosphine palladium (0.58g, 0.5mmol), potassium carbonate (13.8g, 0.1mol), 100mL of toluene, 50mL of ethanol, and 50mL of water was refluxed for 4h to separate the aqueous phase with dichloromethane. 100mL * 3 extraction, combined organic phase, dried over anhydrous sodium sulfate, rotary column chromatography P11-1 16.7g, the yield of 87%.
 

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