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[ CAS No. 1283676-82-3 ] {[proInfo.proName]}

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Chemical Structure| 1283676-82-3
Chemical Structure| 1283676-82-3
Structure of 1283676-82-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1283676-82-3 ]

CAS No. :1283676-82-3 MDL No. :
Formula : C24H26N2O7 Boiling Point : -
Linear Structure Formula :- InChI Key :XKYMEDSRZSGBCL-IBGZPJMESA-N
M.W : 454.47 Pubchem ID :101907290
Synonyms :

Safety of [ 1283676-82-3 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1283676-82-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1283676-82-3 ]

[ 1283676-82-3 ] Synthesis Path-Downstream   1~15

  • 1
  • dimethyl 2-amino-[1,1’-biphenyl]-4,4’-dicarboxylate [ No CAS ]
  • [ 1283676-82-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: dmap; diisopropyl-carbodiimide / dichloromethane / 0.5 h / Cooling with ice 1.2: 40 h / 40 °C 2.1: water; potassium hydroxide / tetrahydrofuran / 16 h / 50 °C
  • 2
  • [ 67-56-1 ]
  • [ 1283676-82-3 ]
  • [ 1283676-80-1 ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid Reflux; optical yield given as %ee;
  • 3
  • [ 67-56-1 ]
  • [ 1283676-82-3 ]
  • C21H22N2O5 [ No CAS ]
  • C21H22N2O5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: C24H26N2O7 With zinc(II) nitrate; N-formyldiethylamine Stage #2: Heating; Stage #3: methanol With sulfuric acid for 16h; Reflux;
  • 4
  • [ 1007568-39-9 ]
  • [ 1283676-82-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol; dichloromethane / 18 h / 2327.23 Torr 2.1: dmap; diisopropyl-carbodiimide / dichloromethane / 0.5 h / Cooling with ice 2.2: 40 h / 40 °C 3.1: water; potassium hydroxide / tetrahydrofuran / 16 h / 50 °C
Multi-step reaction with 3 steps 1.1: acetic acid; iron / 12 h / 50 °C 2.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 96 h / 0 °C / Inert atmosphere 3.1: potassium hydroxide / tetrahydrofuran; water / 19 h / 50 °C 3.2: pH 4
  • 5
  • [ 1283676-80-1 ]
  • [ 1283676-82-3 ]
YieldReaction ConditionsOperation in experiment
88% Stage #1: dimethyl 2-(1-(tert-butoxycarbonyl)pyrrolidine-2-carboxamido)biphenyl-4,4'-dicarboxylate With potassium hydroxide In tetrahydrofuran; water at 50℃; for 19h; Stage #2: With hydrogenchloride In water
393 mg With water; potassium hydroxide In tetrahydrofuran at 50℃; for 16h; optical yield given as %ee;
  • 6
  • [ 1283676-82-3 ]
  • [ 1283676-84-5 ]
YieldReaction ConditionsOperation in experiment
90% With trifluoroacetic acid In dichloromethane for 0.166667h; Cooling with ice;
  • 8
  • 4,4′,4″-(benzene-1,3,5-tricarbonyltris(azanediyl)) tribenzoic acid [ No CAS ]
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 1283676-82-3 ]
  • 4Zn(2+)*O(2-)*C24H24N2O7(2-)*1.33C30H18N3O9(3-)*5H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% at 100℃; for 48h;
  • 9
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 100-21-0 ]
  • [ 1283676-82-3 ]
  • [ 1453220-01-3 ]
  • [Zn4O(1,4-benzenedicarboxylate)1/2(bpdc-ProBoc)1/2(5,5',10,10',15,15'-hexamethyltruxene-2,7,12-tricarboxylato)4/3] [ No CAS ]
YieldReaction ConditionsOperation in experiment
In water at 85℃; for 17h;
  • 10
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 605-70-9 ]
  • [ 1283676-82-3 ]
  • [ 1453220-01-3 ]
  • [Zn4O(ndc)1/2(bpdc-ProBoc)1/2(5,5',10,10',15,15'-hexamethyltruxene-2,7,12-tricarboxylato)4/3] [ No CAS ]
  • 11
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 100-21-0 ]
  • [ 1137578-95-0 ]
  • [ 1283676-82-3 ]
  • [Zn4O(1,4-benzenedicarboxylate)1/2(bpdc-ProBoc)1/2(hett)4/3] [ No CAS ]
YieldReaction ConditionsOperation in experiment
In water at 85℃; for 17h;
  • 12
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 100-21-0 ]
  • [ 1283676-82-3 ]
  • 5,5',10,10',15,15'-hexabutyltruxene-2,7,12-tricarboxylic acid [ No CAS ]
  • [Zn4O(1,4-benzenedicarboxylate)1/2(bpdc-ProBoc)1/2(hbtt)4/3] [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: zinc nitrate tetrahydrate; terephthalic acid; C24H26N2O7; 5,5',10,10',15,15'-hexabutyltruxene-2,7,12-tricarboxylic acid In water at 85℃; for 17h; Stage #2: for 20h;
  • 13
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 100-21-0 ]
  • [ 1283676-82-3 ]
  • 5,5',10,10',15,15'-hexaoctyltruxene-2,7,12-tricarboxylic acid [ No CAS ]
  • [Zn4O(1,4-benzenedicarboxylate)1/2(bpdc-ProBoc)1/2(hott)4/3] [ No CAS ]
YieldReaction ConditionsOperation in experiment
In water at 85℃; for 24h;
  • 14
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 605-70-9 ]
  • [ 1283676-82-3 ]
  • 5,5',10,10',15,15'-hexabutyltruxene-2,7,12-tricarboxylic acid [ No CAS ]
  • [Zn4O(ndc)1/2(bpdc-ProBoc)1/2(hbtt)4/3] [ No CAS ]
  • 15
  • zinc nitrate tetrahydrate [ No CAS ]
  • [ 605-70-9 ]
  • [ 1283676-82-3 ]
  • 5,5',10,10',15,15'-hexaoctyltruxene-2,7,12-tricarboxylic acid [ No CAS ]
  • [Zn4O(ndc)1/2(bpdc-ProBoc)1/2(hott)4/3] [ No CAS ]
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