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Chemical Structure| 1305711-34-5 Chemical Structure| 1305711-34-5

Structure of 1305711-34-5

Chemical Structure| 1305711-34-5

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Product Details of [ 1305711-34-5 ]

CAS No. :1305711-34-5
Formula : C9H11N3O
M.W : 177.20
SMILES Code : NC1=NN(C)C2=C1C(OC)=CC=C2
MDL No. :MFCD13176793
InChI Key :NYVQTRCMCJMRST-UHFFFAOYSA-N
Pubchem ID :75365498

Safety of [ 1305711-34-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362

Application In Synthesis of [ 1305711-34-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1305711-34-5 ]

[ 1305711-34-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 94088-46-7 ]
  • [ 60-34-4 ]
  • [ 1305711-34-5 ]
YieldReaction ConditionsOperation in experiment
91% In ethanol;Reflux; General procedure: A mixture of benzonitrile 1 (10.0 mmol) and methylhydrazine (2.8 mL, 50.0 mmol) in EtOH (10.0 mL) was heated to reflux overnight. The mixture was cooled to rt and then concentrated. H2O (10.0 mL) and EtOAc (20.0 mL) were added to the residue. The organic layer was washed with H2O (10.0 mL), brine (10.0 mL), dried over Na2SO4, filtered, and concentrated in vacuo. The residue was subjected to silica-gel chromatography by using EtOAc/hexanes (1:1) as eluent to give the product 2.
 

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