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Chemical Structure| 1320211-47-9 Chemical Structure| 1320211-47-9

Structure of 1320211-47-9

Chemical Structure| 1320211-47-9

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Product Details of [ 1320211-47-9 ]

CAS No. :1320211-47-9
Formula : C10H6BrN3
M.W : 248.08
SMILES Code : BrC1=NC2=NC3=CC=CC=C3N2C=C1

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Application In Synthesis of [ 1320211-47-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1320211-47-9 ]

[ 1320211-47-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1320211-47-9 ]
  • [ 54288-70-9 ]
  • C15H15BrN4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
67% With triethylamine; In N,N-dimethyl-formamide; at 100℃;Microwave irradiation; To a microwave vial equipped with a magnetic stir bar, containing DMF (1 mL) was 2-bromobenzo[4,5]imidazo[ 1,2-a]pyrimidine (0.067 g, 0.27 mmol, 1.0 equiv), 4-bromopiperidine hydrochloride (0.099 g, 0.405 mmol, 1.5 equiv) and triethylamine (0.113 ml, 0.810 mmol, 3.0 equiv). The suspension was irradiated in a Biotage Initiator microwave reactor (250 W) at 100 °C for 10 min. After cooling to room temperature, the crude product was purifled by HPLC to afford 0.06 g (67percent) of T777P2 as a white solid.
 

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