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Chemical Structure| 13235-60-4 Chemical Structure| 13235-60-4

Structure of 13235-60-4

Chemical Structure| 13235-60-4

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Product Details of [ 13235-60-4 ]

CAS No. :13235-60-4
Formula : C9H6Cl2O3
M.W : 233.05
SMILES Code : O=C(Cl)C1=CC=C(OC)C(C(Cl)=O)=C1
MDL No. :MFCD09954354

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Application In Synthesis of [ 13235-60-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13235-60-4 ]

[ 13235-60-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 443-86-7 ]
  • [ 13235-60-4 ]
  • N<SUP>1</SUP>,N<SUP>3</SUP>-bis(3-fluoro-2-methylphenyl)-4-methoxybenzene-1,3-isophthalamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
67.1% General procedure: The solution of 4-methoxy-1,3-benzenedichloride (6)(0.93 g, 4.0 mmol) in anhydrous THF (15 mL) was added to3-bromine-4-methylaniline (1.48 g, 8.0 mmol). This solutionwas stirred rapidly at room temperature for about 1 hand then pyridine (1 mL) was added. The solution wasrefluxed for 4-8 h. The residue was recrystallized frommethanol-water to terminal compound 1a (1.81 g, yield85.2%). The other compounds (1b-1i) were prepared with thesimilar method of preparing compound 1a.
 

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