Home Cart Sign in  
Chemical Structure| 132997-94-5 Chemical Structure| 132997-94-5

Structure of 132997-94-5

Chemical Structure| 132997-94-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 132997-94-5 ]

CAS No. :132997-94-5
Formula : C7H14O4
M.W : 162.18
SMILES Code : O=CCOCCOCCOC
MDL No. :MFCD24674019

Safety of [ 132997-94-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335-H227
Precautionary Statements:P210-P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P370+P378-P403+P233-P403+P235-P405-P501

Application In Synthesis of [ 132997-94-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 132997-94-5 ]

[ 132997-94-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 132997-94-5 ]
  • [ 498-63-5 ]
  • (1-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethyl}-pyrrolidin-2-yl)-methanol [ No CAS ]
  • 2
  • [ 3684-12-6 ]
  • [ 120329-58-0 ]
  • [ 132997-94-5 ]
  • C80H25NO3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
40% In chlorobenzene; for 72h;Reflux; A chlorobenzene solution (150 mL) of N-phenyl-2-phenylglycine (112 mg, 0.5 mmol), 3,6,9-trioxadecanal(162 mg, 1 mmol), and a fullerene (360 mg, 0.5 mmol) washeated under reflux for 72 hours. The reaction product solution was concentratedunder reduced pressure, and the reaction product was purifiedby colunm chromatography (Si02 , toluene-toluene:ethyl acetate=25:1), followed by further purification byHPLC (Buckyprep: toluene), thereby obtaining 217 mg( 40.0%) of the target product (purity: 99% or more). 1H-NMR (CDC13)o: 3.35 (3H, s), 3.45-3.73 (8H,m), 4.30 (lH, d, 1=10.0 Hz), 4.46 (lH, d-d, 1=10.0, 5.2 Hz),5.87 (lH, d, 1=5.2 Hz), 6.78 (lH, s), 6.95-7.05 (lH, m),7.15-7.40 (7H, m), 7.70 (2H, d, 1=8.0 Hz). MS (FAB) m/z 1047(M+ ). HRMS calcd forC80H26N03(M+1) 1048.1913; found 1048.1897.
 

Historical Records