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Chemical Structure| 134575-11-4 Chemical Structure| 134575-11-4

Structure of 134575-11-4

Chemical Structure| 134575-11-4

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Product Details of [ 134575-11-4 ]

CAS No. :134575-11-4
Formula : C18H26N2O2
M.W : 302.42
SMILES Code : [H][C@]12CN(CC3=CC=CC=C3)C[C@@]1([H])[C@@H]2CNC(OC(C)(C)C)=O
MDL No. :MFCD23378529

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Application In Synthesis of [ 134575-11-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 134575-11-4 ]

[ 134575-11-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 134575-11-4 ]
  • [ 134575-12-5 ]
YieldReaction ConditionsOperation in experiment
With hydrogen;palladium dihydroxide; In methanol; under 1034.32 Torr; for 10.0h; Step 5: The carbamate (i) (1.9 g, 6.3 mmol) prepared in step 4 wasdissolved in methanol (100 ml) and mixed with palladium hydroxide (20%, 0.4 g).The mixture was transferred to a Parr bottle, which was then charged withhydrogen to a pressure of 20 psi. The Parr bottle was shaken for 10 h. Theremaining hydrogen was removed from the Parr bottle under vacuum, and thereaction was filtered through Celite (diatomaceous earth). The filtrate was thenconcentrated to provide pure amine B (1.4 g).
 

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