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Chemical Structure| 1350550-50-3 Chemical Structure| 1350550-50-3

Structure of 1350550-50-3

Chemical Structure| 1350550-50-3

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Product Details of [ 1350550-50-3 ]

CAS No. :1350550-50-3
Formula : C12H22BrNO2
M.W : 292.21
SMILES Code : O=C(OC(C)(C)C)NC1CCC(CBr)CC1

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Application In Synthesis of [ 1350550-50-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1350550-50-3 ]

[ 1350550-50-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1306829-95-7 ]
  • [ 1350550-50-3 ]
  • [ 1350550-40-1 ]
YieldReaction ConditionsOperation in experiment
85% A 10 n L microwave tube was charged with 3-bromo-6-(methylthio)-lH- pyrazolo[3,4-d]pyrimidine (0.2 g, 0.8 mmol), potassium carbonate (0.34 g, 2.4 mmol), and DMSO (1.5 mL). The resulting mixture was stirred for 20 min, then tert-butyl trans-4- (bromomethyl)cyclohexylcarbamate (0.29 g, 1.0 mmol) and THF (3 mL) were added. The resulting mixture was heated at 150 C for 10 min in microwave, The reaction mixture was poured into water and extracted with Et20 (3X). The combined ether layers were dried (Na2S04), concentrated, and purified by Isco to give ieri-Butyl-4-((3-bromo-6-(methylthio)- lH-pyrazolo[3,4-d]pyrimidin-l-yl)methyl) cyclohexyl carbamate (0,31 g, 85%) as a white solid. MS m/z 478.1 [M+Na]+
  • 2
  • [ 1306829-95-7 ]
  • [ 1350550-50-3 ]
  • C18H26BrN5O2S [ No CAS ]
  • tert-butyl trans-4-((3-bromo-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidin-1-yl)methyl)cyclohexylcarbamate [ No CAS ]
 

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