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Chemical Structure| 13519-74-9 Chemical Structure| 13519-74-9

Structure of 13519-74-9

Chemical Structure| 13519-74-9

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Product Details of [ 13519-74-9 ]

CAS No. :13519-74-9
Formula : C8H10ClN
M.W : 155.62
SMILES Code : CCNC1=CC=CC=C1Cl
MDL No. :MFCD00792552

Safety of [ 13519-74-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319
Precautionary Statements:P501-P261-P270-P271-P264-P280-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330-P302+P352+P312-P304+P340+P312

Application In Synthesis of [ 13519-74-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13519-74-9 ]

[ 13519-74-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 103-69-5 ]
  • [ 13519-74-9 ]
  • [ 13519-75-0 ]
YieldReaction ConditionsOperation in experiment
With trichloroisocyanuric acid; scandium tris(trifluoromethanesulfonate); In toluene; at 90℃; for 12h; In an air atmosphere, scandium triflate (5mol%, 4.9mg), N-ethylaniline (0.2mmol, 24.2mg),Trichloroisocyanuric acid (0.07mmol, 16.3mg) and a magnetic stir bar were added to a 35mL glass pressure tube.Toluene (4 mL) was then added, and the reaction tube was reacted at 90C for 12 hours. After the reaction is completed, the reaction system is cooled to room temperature,Open the reaction vessel at room temperature, add 10 mL of water; extract with 30 mL of dichloromethane, collect the organic phase, dry the organic phase with anhydrous sodium sulfate, and purify the organic layer by column chromatography to obtain a pure product with a yield of 77%.The gas phase selectivity of the ortho and para positions is o:p=84:16.
 

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