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[ CAS No. 1354960-91-0 ] {[proInfo.proName]}

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Chemical Structure| 1354960-91-0
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Product Details of [ 1354960-91-0 ]

CAS No. :1354960-91-0 MDL No. :MFCD24039170
Formula : C8H7FO3 Boiling Point : -
Linear Structure Formula :- InChI Key :VMJGSRHNSMLVHG-UHFFFAOYSA-N
M.W : 170.14 Pubchem ID :46831649
Synonyms :

Safety of [ 1354960-91-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1354960-91-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1354960-91-0 ]

[ 1354960-91-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 700-85-6 ]
  • [ 1354960-91-0 ]
YieldReaction ConditionsOperation in experiment
83% To a solution of 5-fluoro-2-benzofuran-1 (3H)-one (0.235 g, 0.00154 mol) in methanol (2.50 mL) and water (2.50 mL) was added potassium hydroxide (0.500 g, 0.00891 mol) and the reaction mixture was stirred at 50 C. under nitrogen for 2 hours. The reaction was diluted with an aqueous solution of hydrochloric acid (2.0 M, 10.0 mL). The aqueous layer was then extracted twice with ethyl acetate (2×15 mL). The organic layers were combined, then dried over sodium sulfate, filtered and concentrated in vacuo. The title compound was obtained after trituration in dichloromethane (8.0 mL) as a white solid (0.218 g, 0.00128 mol, 83% yield).LCMS Rt=0.79 minutes MS m/z 169 [M-H]-1H NMR (400 MHz, d6-DMSO): delta 4.82 (s, 2H), 7.12-7.17 (m, 1H), 7.43-7.47 (m, 1H), 7.91-7.95 (q, 1H)
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