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Chemical Structure| 1372775-52-4 Chemical Structure| 1372775-52-4

Structure of 1372775-52-4

Chemical Structure| 1372775-52-4

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Product Details of [ 1372775-52-4 ]

CAS No. :1372775-52-4
Formula : C24H19N
M.W : 321.41
SMILES Code : C1(C2=CC=CC=C2)=CC=CC=C1NC3=CC=C(C4=CC=CC=C4)C=C3
MDL No. :MFCD22988894

Safety of [ 1372775-52-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313

Application In Synthesis of [ 1372775-52-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1372775-52-4 ]

[ 1372775-52-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50548-45-3 ]
  • [ 1372775-52-4 ]
  • C36H25NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
53% With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; for 5h;Inert atmosphere; Reflux; To a 500 ml round bottom flask in a nitrogen atmosphereCompound 1-Bromobenzofuran (10.0 g, 40.65 mmol),Di ([1,1'-biphenyl] -4-yl) amine(di ([1,1'-biphenyl] -4-yl) amine) (14.35 g, 44.72 mmol)Xylene(Xylene) After dissolving, sodium tert-butoxide(sodium tert-butoxide) (5.08 g, 52.85 mol), And bis (tri-tert-butylphosphine) palladium (0)(Bis (tri-tert-butylphosphine) palladium (0)) (0.21 g, 0.41 mmol) was added and the mixture was heated with stirring for 5 hours.After lowering the temperature to room temperature and removing the salt by filtration, the xylene was concentrated under reduced pressure, and tetrahydrofuran: hexAcid = 1: 25, to obtain Compound 2 (10.47 g, yield: 53percent).
 

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