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CAS No. : | 1373432-11-1 | MDL No. : | MFCD31707596 |
Formula : | C20H25O3P | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 344.38 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; chlorobenzene / 1 h / -78 °C / Inert atmosphere 1.2: -78 - 20 °C / Inert atmosphere 2.1: titanium(IV) isopropylate / tetrahydrofuran / 12 h / Inert atmosphere; Reflux |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
95% | With titanium(IV) isopropylate In tetrahydrofuran at 70℃; for 16h; Inert atmosphere; stereospecific reaction; | |
90% | With titanium(IV) isopropylate In tetrahydrofuran for 12h; Inert atmosphere; Reflux; | |
With titanium(IV) isopropylate In tetrahydrofuran Inert atmosphere; stereospecific reaction; |
With titanium(IV) isopropylate In tetrahydrofuran at 65℃; for 14h; Inert atmosphere; Schlenk technique; | ||
With trichlorosilane; triethylamine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride / 1,4-dioxane / Inert atmosphere 2: lithium diisopropyl amide / Inert atmosphere 3: titanium(IV) isopropylate / tetrahydrofuran / Inert atmosphere |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: lithium diisopropyl amide / Inert atmosphere 2: titanium(IV) isopropylate / tetrahydrofuran / Inert atmosphere | ||
Multi-step reaction with 2 steps 1: lithium diisopropyl amide 2: trichlorosilane; triethylamine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: tris-(dibenzylideneacetone)dipalladium(0); potassium fluoride / 1,4-dioxane / Inert atmosphere 2: lithium diisopropyl amide / Inert atmosphere 3: titanium(IV) isopropylate / tetrahydrofuran / Inert atmosphere |
A1005935[ 1477517-18-2 ]
(2R,3R)-3-(tert-Butyl)-4-(2,6-dimethoxyphenyl)-2-methyl-2,3-dihydrobenzo[d][1,3]oxaphosphole
Reason: Optical isomers