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Chemical Structure| 13928-68-2 Chemical Structure| 13928-68-2

Structure of 13928-68-2

Chemical Structure| 13928-68-2

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Product Details of [ 13928-68-2 ]

CAS No. :13928-68-2
Formula : C14H20O4
M.W : 252.31
SMILES Code : O=C(C12CC3(C(O)=O)CC(C2)(C)CC(C3)(C)C1)O
MDL No. :MFCD01825788

Safety of [ 13928-68-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 13928-68-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13928-68-2 ]

[ 13928-68-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 702-79-4 ]
  • [ 201230-82-2 ]
  • [ 13928-68-2 ]
YieldReaction ConditionsOperation in experiment
60% General procedure: At room temperature, CBr4·2AlBr3 was prepared by stirring CBr4 with AlBr3 in a molar ratio of 1-2 in anhydrous CH2Br2. Next, at 0 C under atmospheric CO pressure, AdH (1) (1.43 mmol) was added to the freshly prepared CBr4·2AlBr3 (2.87 mmol) in CH2Br2 (3 mL). The mixture was stirred for 3 h. Then at atmospheric CO pressure, H2O (15 mL) was added carefully with cooling. The reaction mixture was kept for 1-2 d until the precipitation of 1,3-Ad(COOH)2 was complete. The Ad(COOH)2 was filtered, washed with H2O, dried, and crystallized from AcOH. The yield of analytically pure compound was 80% with respect to 1.
  • 2
  • [ 64-18-6 ]
  • [ 702-79-4 ]
  • [ 13928-68-2 ]
 

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