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[ CAS No. 1398398-12-3 ] {[proInfo.proName]}

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Chemical Structure| 1398398-12-3
Chemical Structure| 1398398-12-3
Structure of 1398398-12-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1398398-12-3 ]

CAS No. :1398398-12-3 MDL No. :N/A
Formula : C24H41BO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 372.39 Pubchem ID :-
Synonyms :

Safety of [ 1398398-12-3 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:
Hazard Statements:H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1398398-12-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1398398-12-3 ]

[ 1398398-12-3 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 1398398-12-3 ]
  • [ 67061-69-2 ]
  • [ 1446140-70-0 ]
  • 2
  • [ 61676-62-8 ]
  • [ 126930-72-1 ]
  • [ 1398398-12-3 ]
  • 3
  • [ 1000623-95-9 ]
  • [ 1398398-12-3 ]
  • [ 1442482-76-9 ]
  • 4
  • [ 126930-72-1 ]
  • [ 73183-34-3 ]
  • [ 1398398-12-3 ]
YieldReaction ConditionsOperation in experiment
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate;Inert atmosphere; Reflux; <strong>[126930-72-1]1-bromo-4-dodecylbenzene</strong> (5.0 g, 15.4 mmol, 1.0 eq.), bispinacolato diboron (4.7 g, 1.2 eq.), potassium acetate (4.5 g, 3 eq.), and a bis(diphenylphosphino) ferrocene-palladium(II) dichloride dichloromethane complex (0.38 g, 0.03 eq.) were weighed and put into a 200 mL three-necked round bottom flask. Degassing under reduced pressure and nitrogen purge were sufficiently performed. Thereafter, 50 mL of cyclopentyl methyl ether was added thereto in a nitrogen atmosphere, and the mixture was refluxed and stirred. After completion of the reaction, heating was stopped, and the temperature of the reaction liquid was returned to room temperature. Extraction was performed with toluene, the organic solvent layers were then unified, anhydrous sodium sulfate was added thereto, and the mixture was allowed to stand for a while. Sodium sulfate was filtered off, and the solution was concentrated under reduced pressure. The mixture containing a desired product was further caused to pass through an activated carbon column chromatography, and a fraction containing a desired product was collected and concentrated under reduced pressure. Thus, a desired product ?PC12Bpin? was obtained.
  • 5
  • [ 1398398-12-3 ]
  • [ 55120-48-4 ]
  • [ 2196202-99-8 ]
YieldReaction ConditionsOperation in experiment
63% With tetrakis(triphenylphosphine) palladium(0); Aliquat 336; potassium carbonate In water; toluene at 110℃; for 48h; Inert atmosphere;
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