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Chemical Structure| 13991-01-0 Chemical Structure| 13991-01-0

Structure of 13991-01-0

Chemical Structure| 13991-01-0

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Product Details of [ 13991-01-0 ]

CAS No. :13991-01-0
Formula : C16H17NO
M.W : 239.31
SMILES Code : O=C(C1=CC=C(CN(C)C)C=C1)C2=CC=CC=C2
MDL No. :N/A

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Application In Synthesis of [ 13991-01-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13991-01-0 ]

[ 13991-01-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13991-01-0 ]
  • [ 4263-52-9 ]
  • C18H21NO4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
70.1 g In tetrahydrofuran; at 20℃; for 6h; 0.2 mol of compound (6) was weighed and added to a round bottom flask with mechanical stirring. 0.2 mol of sodium 2-bromoethanesulfonate BrCH2CH2SO3Na dissolved in 400 mL of anhydrous THF was added dropwise at 20 C. After the completion of the dropwise addition, the reaction was continued for 6 hours to obtain a white precipitate, which was purified by centrifugation several times to obtain 70.1 g of an amphoteric ion-based antibacterial compound. The reaction formula was as follows: (0160) The nuclear magnetic data of the antibacterial hydrophilic compound obtained in some embodiments was as follows: 1H NMR (CD3Cl, 600 MHz, TMS), delta (ppm) 7.86 (d, 2H), 7.79 (d, 2H), 7.74 (d, 2H), 7.58 (t, 1H), 7.46 (t, 2H), 3.73 (s, 6H), 3.40 (m, 2H), 3.0 (m, 2H). 13C-NMR (CD3Cl, 600 MHz). delta(ppm) [195.7, 150.2, 139.6, 133.3, 133.1, 131.4, 130.4, 128.5, 120.9, 67.2, 52.4, 49.6, 46.0].
 

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