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Chemistry
Organic Building Blocks
Amines
1-(Dimethylamino)-2-methylpropan-2-ol
Chemistry
Organic Building Blocks
Amines
Alcohols Aliphatic Chain Hydrocarbons

[ CAS No. 14123-48-9 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
3d Animation Molecule Structure of 14123-48-9
Chemical Structure| 14123-48-9
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Quality Control of [ 14123-48-9 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 14123-48-9 ]

Product Details of [ 14123-48-9 ]

CAS No. :14123-48-9 MDL No. :MFCD11934288
Formula : C6H15NO Boiling Point : -
Linear Structure Formula :- InChI Key :XTYRIICDYQTTTC-UHFFFAOYSA-N
M.W : 117.19 Pubchem ID :9793738
Synonyms :

Calculated chemistry of [ 14123-48-9 ]

Physicochemical Properties

Num. heavy atoms : 8
Num. arom. heavy atoms : 0
Fraction Csp3 : 1.0
Num. rotatable bonds : 2
Num. H-bond acceptors : 2.0
Num. H-bond donors : 1.0
Molar Refractivity : 35.05
TPSA : 23.47 Ų

Pharmacokinetics

GI absorption : High
BBB permeant : No
P-gp substrate : No
CYP1A2 inhibitor : No
CYP2C19 inhibitor : No
CYP2C9 inhibitor : No
CYP2D6 inhibitor : No
CYP3A4 inhibitor : No
Log Kp (skin permeation) : -6.87 cm/s

Lipophilicity

Log Po/w (iLOGP) : 2.01
Log Po/w (XLOGP3) : 0.2
Log Po/w (WLOGP) : 0.32
Log Po/w (MLOGP) : 0.61
Log Po/w (SILICOS-IT) : -0.16
Consensus Log Po/w : 0.59

Druglikeness

Lipinski : 0.0
Ghose : None
Veber : 0.0
Egan : 0.0
Muegge : 1.0
Bioavailability Score : 0.55

Water Solubility

Log S (ESOL) : -0.56
Solubility : 32.2 mg/ml ; 0.275 mol/l
Class : Very soluble
Log S (Ali) : -0.25
Solubility : 65.7 mg/ml ; 0.56 mol/l
Class : Very soluble
Log S (SILICOS-IT) : -0.59
Solubility : 30.1 mg/ml ; 0.256 mol/l
Class : Soluble

Medicinal Chemistry

PAINS : 0.0 alert
Brenk : 0.0 alert
Leadlikeness : 1.0
Synthetic accessibility : 1.0

Safety of [ 14123-48-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P342+P311-P305+P351+P338 UN#:N/A
Hazard Statements:H319-H315-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 14123-48-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14123-48-9 ]

[ 14123-48-9 ] Synthesis Path-Downstream   1~84

  • 1
  • [ 558-30-5 ]
  • [ 124-40-3 ]
  • [ 71-43-2 ]
  • [ 14123-48-9 ]
Reference： [1]Patent: DE199148,
  • 2
  • [ 558-30-5 ]
  • [ 124-40-3 ]
  • [ 14123-48-9 ]
Reference： [1]European Journal of Inorganic Chemistry,2015,vol. 2015,p. 2323 - 2329
[2]Bulletin des Sciences Pharmacologiques,1930,vol. 37,p. 242
    Chemisches Zentralblatt,1931,vol. 102,p. 812
[3]ChemSusChem,2019,vol. 12,p. 4211 - 4220
  • 3
  • [ 14254-57-0 ]
  • [ 14123-48-9 ]
  • isonicotinic acid-(dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Helvetica Chimica Acta,1947,vol. 30,p. 507,513
  • 4
  • [ 917-64-6 ]
  • [ 15364-56-4 ]
  • [ 14123-48-9 ]
Reference： [1]Patent: DE169819,
  • 5
  • [ 917-64-6 ]
  • [ 63989-57-1 ]
  • [ 14123-48-9 ]
Reference： [1]Patent: DE169819,
  • 6
  • [ 60-29-7 ]
  • [ 14123-48-9 ]
  • [ 925-90-6 ]
  • [ 124-40-3 ]
  • [ 78-84-2 ]
Reference： [1]Journal of the American Chemical Society,1938,vol. 60,p. 1375
  • 7
  • [ 14123-48-9 ]
  • benzoic acid-(dimethylamino-<i>tert</i>-butyl ester) [ No CAS ]
Reference： [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1904,vol. 138,p. 767
  • 8
  • [ 14123-48-9 ]
  • [ 108-24-7 ]
  • acetic acid-(dimethylamino-<i>tert</i>-butyl ester) [ No CAS ]
Reference： [1]Proceedings of the Indiana Academy of Science,1949,vol. 58,p. 120,123
  • 9
  • [ 14123-48-9 ]
  • [ 102-92-1 ]
  • <i>trans</i>-cinnamic acid-(dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Patent: DE169787,
  • 10
  • [ 14123-48-9 ]
  • [ 122-04-3 ]
  • 4-nitro-benzoic acid-(4-dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Bulletin des Sciences Pharmacologiques,1930,vol. 37,p. 242
    Chemisches Zentralblatt,1931,vol. 102,p. 812
  • 11
  • [ 558-42-9 ]
  • [ 124-40-3 ]
  • [ 14123-48-9 ]
Reference： [1]Journal of the American Chemical Society,1938,vol. 60,p. 1375
[2]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1904,vol. 138,p. 767
[3]Patent: DE169746,
  • 12
  • [ 50-00-0 ]
  • [ 75-86-5 ]
  • [ 67622-86-0 ]
  • [ 14123-48-9 ]
Reference： [1]Patent: US2462736,1944,
  • 13
  • [ 14123-48-9 ]
  • [ 814-68-6 ]
  • [ 45021-14-5 ]
Reference： [1]Journal of the American Chemical Society,1959,vol. 81,p. 3618,3620
  • 14
  • [ 14123-48-9 ]
  • [ 108-12-3 ]
  • isovaleric acid-(dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Patent: DE169787,
  • 15
  • [ 14123-48-9 ]
  • [ 121-90-4 ]
  • 3-nitro-benzoic acid-(dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Bulletin des Sciences Pharmacologiques,1930,vol. 37,p. 242
    Chemisches Zentralblatt,1931,vol. 102,p. 812
  • 16
  • [ 14123-48-9 ]
  • [ 610-14-0 ]
  • 2-nitro-benzoic acid-(dimethylamino-<i>tert</i>-butyl ester); hydrochloride [ No CAS ]
Reference： [1]Bulletin des Sciences Pharmacologiques,1930,vol. 37,p. 242
    Chemisches Zentralblatt,1931,vol. 102,p. 812
  • 17
  • [ 558-42-9 ]
  • [ 75-50-3 ]
  • [ 14123-48-9 ]
Reference： [1]Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences,1904,vol. 138,p. 767
  • 18
  • [ 14123-48-9 ]
  • [ 74-88-4 ]
  • (β-hydroxy-isobutyl)-trimethyl-ammonium; iodide [ No CAS ]
Reference： [1]Chemisches Zentralblatt,1910,vol. 81,p. 1365
  • 19
  • [ 75-44-5 ]
  • [ 14123-48-9 ]
  • [ 69146-72-1 ]
Reference： [1]Journal of Medicinal Chemistry,1979,vol. 22,p. 191 - 195
  • 20
  • [ 1871-76-7 ]
  • [ 14123-48-9 ]
  • 1,1-Dimethyl-2-dimethylaminoethyl-diphenylacetat [ No CAS ]
Reference： [1]European Journal of Medicinal Chemistry,1975,vol. 10,p. 450 - 452
  • 21
  • [ 14123-50-3 ]
  • [ 14123-48-9 ]
Reference： [1]Journal of Organic Chemistry,1967,vol. 32,p. 3607 - 3613
  • 22
  • [ 14123-48-9 ]
  • [ 108-24-7 ]
  • [ 74-88-4 ]
  • [ 35437-96-8 ]
Reference： [1]Journal of medicinal chemistry,1970,vol. 13,p. 299 - 301
  • 23
  • [ 5395-71-1 ]
  • [ 14123-48-9 ]
  • (2-Ethoxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 24
  • [ 14123-48-9 ]
  • [ 32223-62-4 ]
  • (2-Propoxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 25
  • [ 14123-48-9 ]
  • [ 55792-33-1 ]
  • (2-Butoxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 26
  • [ 14123-48-9 ]
  • [ 32223-65-7 ]
  • (2-Pentyloxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 27
  • [ 14123-48-9 ]
  • [ 32223-68-0 ]
  • (2-Hexyloxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 28
  • [ 14123-48-9 ]
  • [ 32349-77-2 ]
  • (2-Octyloxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 29
  • [ 14123-48-9 ]
  • [ 55792-35-3 ]
  • (2-Heptyloxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 31
  • [ 14123-48-9 ]
  • [ 700-87-8 ]
  • (2-Methoxy-phenyl)-carbamic acid 2-dimethylamino-1,1-dimethyl-ethyl ester [ No CAS ]
Reference： [1]Il Farmaco,1992,vol. 47,p. 327 - 334
  • 32
  • [ 124763-30-0 ]
  • [ 14123-48-9 ]
  • p-(125I)iodophenoxyacetic acid [ No CAS ]
Reference： [1]Chemical and Pharmaceutical Bulletin,1989,vol. 37,p. 2282 - 2286
  • 34
  • [ 124-40-3 ]
  • dimethylethylene oxide [ No CAS ]
  • [ 14123-48-9 ]
Reference： [1]Patent: DE199148,
YieldReaction ConditionsOperation in experiment
Erhitzen des Reaktionsprodukts auf 280-420grad;
  • 36
  • [ 14123-48-9 ]
  • [ 7664-93-9 ]
  • [ 124-40-3 ]
  • [ 78-84-2 ]
Reference： [1]Campbell; Campbell [Journal of the American Chemical Society, 1938, vol. 60, p. 1375]
  • 37
  • 3-[1,3]dioxolo[4,5-<i>g</i>]quinolin-8-yl-2-(2-iodo-4,5-dimethoxy-phenyl)-acryloyl chloride [ No CAS ]
  • [ 14123-48-9 ]
  • 3-(6,7-methylenedioxyquinolin-4-yl)-2-(2-iodo-4,5-dimethoxyphenyl)acrylic acid 2-(N,N-dimethylamino)-1,1-dimethylethyl ester [ No CAS ]
Reference： [1]Bioorganic and Medicinal Chemistry,2005,vol. 13,p. 6782 - 6794
  • 38
  • [ 14123-48-9 ]
  • [ 126485-78-7 ]
Reference： [1]Chemical and Pharmaceutical Bulletin,1989,vol. 37,p. 2276 - 2281
  • 39
  • [ 14123-48-9 ]
  • [ 100536-64-9 ]
Reference： [1]Journal of the American Chemical Society,1959,vol. 81,p. 3618,3620
  • 40
  • [ 14123-48-9 ]
  • [ 69146-63-0 ]
Reference： [1]Journal of Medicinal Chemistry,1979,vol. 22,p. 191 - 195
  • 41
  • [ 786689-27-8 ]
  • [ 14123-48-9 ]
  • N-[3-chloro-4-(pyridin-2-ylmethoxy)phenyl]-5-[2-(dimethylamino)-1,1-dimethylethoxy]quinazolin-4-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
45% With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In dichloromethane; at 20℃; for 4 - 5h; DI-TERT-BUTYL HYDRAZODICARBOXYLATE (64 mg, 0.28 mmol) was added to a mixture of 4- (3-CHLORO-4- (2-PYRIDYLMETHOXY) anilino) -5-hydroxyquinazoline (prepared as described in Example 14, preparation of starting materials, 70 mg, 0.19 mmol), 2- (dimethylamino)-2- METHYLPROPAN-1-OL (33 mg, 0. 28 mmol) and triphenylphosphine (73 mg, 0. 28 mmol) in anhydrous DCM (15 ml). The mixture was stirred at ambient temperature. At intervals of 1 hour and 2 hours, further charges of 2- (DIMETHYLAMINO)-2-METHYLPROPAN-L-OL (33 mg, 0.28 mmol), triphenylphosphine (73 mg, 0.28 mmol) and di-tert-butyl hydrazodicarboxylate (64 mg, 0.28 mmol) were made. After 3 hours, the reaction mixture was loaded onto an SCX column. The column was eluted with 20% MEOH in DCM, then with 20 % (7N NH3 in MEOH) in DCM. The product containing fractions were combined and evaporated. The residue was purified by chromatography, eluting with 1% to 3% (10: 1 MEOH/CONC. NH3 (aq)) in DCM. Evaporation of the appropriate fractions and crystallisation of the residue from ethyl acetate/iso-hexane gave the title compound as a white crystalline solid (40 mg, 45% yield); NMR spectrum (DMSO-d6) ; 1.45 (s, 6H), 2.18 (s, 6H), 2.69 (s, 2H), 5.31 (s, 2H), 7.29 (d, 1H), 7.31 (d, 1H), 7.38 (dd, 1H), 7.45 (d, 1H), 7.46 (dd, 1H), 7.59 (d, 1H), 7.71 (dd, 1H), 7.75 (d, 1H), 7.89 (ddd, 1H), 8.40 (s, 1H), 8.60 (d, 1H), 10.76 (s, 1H) ; Mass spectrum MET 478.
Reference： [1]Patent: WO2004/93880,2004,A1 .Location in patent: Page/Page column 118
  • 42
  • [ 14123-48-9 ]
  • [ 1184-54-9 ]
  • bis(dimethylamino-2-methyl-2-propoxy)copper(II) [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% In toluene; for 18h;Heating / reflux; 1.25 g (9.98 mmol) of Cu(OMe)2 was suspended in 50 mL of toluene in a 125 mL Schlenk flask and 2.35 g (20.05 mmol) of dimethylamino-2-methyl-2-propanol was slowly added thereto. The color of the mixed solution gradually changed to dark purple. The dark purple mixture was refluxed for 18 hours under a nitrogen atmosphere and filtered. The resulting filtrate was distilled in a vacuum to remove the solvent. The solid obtained was purified by sublimation at 40 C. under a reduced pressure of 10-2 Torr, to give 2.4 g of the title compound in the form of a dark purple solid having a melting point of 80-90 C. (yield: 82%).Elemental analysis: Calculated for C12H28N2O2Cu: C, 48.71; H, 9.54; N, 9.47. Found: C, 47.39; H, 9.75; N, 9.17.FTIR (cm-1, KBr pellet): nu(M-O) 537, 500, 430 (see FIG. 1).Mass spectrometry (EI, 70 eV), m/z (ion, relative intensity): 295 ([Cu(L)2]+, 9), 237 ([Cu(L)2-CH2NMe2]+, 37), 222 ([Cu(L)2-CH2NMe2-Me]+, 9), 179 ([Cu(L)]+, 34), 164 ([Cu(L)-Me]+, 17), 58 ([CH2NMe2]+, 100).
Reference： [1]Patent: US6982341,2006,B1 .Location in patent: Page/Page column 4
  • 43
  • [ 546-68-9 ]
  • [ 14123-48-9 ]
  • C24H56N4O4Ti [ No CAS ]
YieldReaction ConditionsOperation in experiment
48% In xylene; at 135℃; for 18h; Into a reaction flask were dropped 0.100 mol of tetra(2-propoxy)titanium, 60 ml of dehydrated xylene, and 0.440 mol of <strong>[14123-48-9]1-dimethylamino-2-methyl-2-propanol</strong> and allowed to react at 135C for 18 hours in a dry argon atmosphere while removing by-produced 2-propanol by evaporation. Xylene was removed by evaporation, and the residue was distilled under reduced pressure. A pale yellow liquid was obtained from the fraction at 5 to 7 Pa and a tower top temperature of 122 to 124C in a yield of 48%. The pale yellow liquid was purified by distillation under reduced pressure to obtain a liquid. The recovery of the purification was 94%. The resulting liquid was identified to be the title compound, compound No. 13. The results of analyses on the liquid are shown below. Results of analyses: (1) Elemental analysis (metal analysis: ICP-AES) Ti: 9.43% by mass (calcd.: 9.34%) (2) 1H-NMR (solvent: deuterobenzene) (chemical shift: multiplicity:number of hydrogens) (1.50:s:24) (2.36:s:24) (2.48:s:8) (3) TG-DTA (Ar: 100 ml/min; temperature rise: 10C/min; amount of sample: 6.175 mg) 50% mass loss temperature: 239C
Reference： [1]Patent: EP1698614,2006,A1 .Location in patent: Page/Page column 8
  • 44
  • [ 14717-56-7 ]
  • [ 14123-48-9 ]
  • C24H56N4O4Zr [ No CAS ]
YieldReaction ConditionsOperation in experiment
53% In xylene; at 135℃; for 10h; Into a reaction flask were dropped 0.100 mol of Zirconium(IV) isopropoxide isopropanol complex, 60 ml of dehydrated xylene, and 0.440 mol of <strong>[14123-48-9]1-dimethylamino-2-methyl-2-propanol</strong> and allowed to react at 135C for 10 hours in a dry argon atmosphere while removing by-produced 2-propanol by evaporation. Xylene was removed by evaporation, and the residue was distilled under reduced pressure. A colorless liquid was obtained from the fraction at 8 to 10 Pa and a tower top temperature of 139 to 140C in a yield of 53%. The colorless liquid was purified by distillation under reduced pressure to obtain a liquid. The recovery of the purification was 92%. The resulting liquid was identified to be the title compound, compound No. 25. The results of analyses on the liquid are shown below. Results of analyses: (1) Elemental analysis (metal analysis: ICP-AES) Zr: 16.8% by mass (calcd.: 16.4%) (2) 1H-NMR (solvent: deuterobenzene) (chemical shift: multiplicity:number of hydrogens) (1.45:s:24) (2.37:s:24) (2.53:s:8) (3) TG-DTA (Ar: 100 ml/min; temperature rise: 10C/min; amount of sample: 7.975 mg) 50% mass loss temperature: 242C
Reference： [1]Patent: EP1698614,2006,A1 .Location in patent: Page/Page column 8
  • 45
  • [ 14123-48-9 ]
  • [ 3236-82-6 ]
  • C14H34NNbO5 [ No CAS ]
Reference： [1]Patent: WO2006/49059,2006,A1 .Location in patent: Page/Page column 11-12
  • 46
  • [ 14123-48-9 ]
  • [ 150747-55-0 ]
  • C14H34NO5Ta [ No CAS ]
Reference： [1]Patent: WO2006/49059,2006,A1 .Location in patent: Page/Page column 10
  • 47
  • iron(III) chloride [ No CAS ]
  • [ 14123-48-9 ]
  • 3C6H14NO(1-)*Fe(3+) [ No CAS ]
Reference： [1]Patent: WO2006/43418,2006,A1 .Location in patent: Page/Page column 13-15
  • 48
  • [ 14123-48-9 ]
  • [ 103729-96-0 ]
  • [ 557-20-0 ]
  • Zn(C2H5)ON(CH3)2CH2C(CH3)2 [ No CAS ]
  • (C10H16)(N(CH3)2)OZnC2H5 [ No CAS ]
  • Zn2(C2H5)2O2N2(CH3)4(C4H8)2 [ No CAS ]
  • Zn2(C2H5)2O2N2(CH3)4(C4H8)(C10H16) [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 49
  • [ 14123-48-9 ]
  • [ 103729-96-0 ]
  • [ 544-97-8 ]
  • Zn2(CH3)2O2N2(CH3)4(C4H8)2 [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 50
  • [ 14123-48-9 ]
  • [ 103729-96-0 ]
  • [ 544-97-8 ]
  • Zn2(CH3)2O2N2(CH3)4(C4H8)(C10H16) [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 51
  • [ 14123-48-9 ]
  • [ 103729-96-0 ]
  • [ 544-97-8 ]
  • Zn2(CH3)2O2N2(CH3)4(C4H8)(C10H16) [ No CAS ]
  • Zn2(CH3)2O2N2(CH3)4(C10H16)2 [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 52
  • [ 14123-48-9 ]
  • [ 557-20-0 ]
  • Zn2(C2H5)2O2N2(CH3)4(C4H8)2 [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 53
  • [ 14123-48-9 ]
  • [ 544-97-8 ]
  • Zn2(CH3)2O2N2(CH3)4(C4H8)2 [ No CAS ]
Reference： [1]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
[2]Journal of the American Chemical Society,1995,vol. 117,p. 4832 - 4842
  • 54
  • Lu(N(SiMe3)2)3 [ No CAS ]
  • [ 14123-48-9 ]
  • Lu(3+)*3OC(CH3)2CH2N(CH3)2(1-)=Lu(OC(CH3)2CH2N(CH3)2)3 [ No CAS ]
Reference： [1]Inorganic Chemistry,1997,vol. 36,p. 3545 - 3552
  • 55
  • bis(trimethylsilyl)amide yttrium(III) [ No CAS ]
  • [ 14123-48-9 ]
  • Y(3+)*3OC(CH3)2CH2N(CH3)2(1-)=Y(OC(CH3)2CH2N(CH3)2)3 [ No CAS ]
Reference： [1]Inorganic Chemistry,1997,vol. 36,p. 3545 - 3552
  • 56
  • [ 14123-48-9 ]
  • [ 1184-54-9 ]
  • [ 756481-76-2 ]
Reference： [1]Inorganic Chemistry Communications,2004,vol. 7,p. 463 - 466
  • 57
  • [ 14123-48-9 ]
  • [ 55147-78-9 ]
  • (dimethylamino-2-methyl-2-propoxy)Sn(II) [ No CAS ]
YieldReaction ConditionsOperation in experiment
In hexane; at 20℃;Product distribution / selectivity; SnCl2 (1 g, 5.27 mmol) and Lithium bistrimethylsilylamide[Li(btsa)] (1.76 g, 10.54 mmol) were added in 250 mL Schlenk flask at room temperature, to which ether (50 mL) was added, followed by stirring for 3 hours. The mixed solution was filtered to eliminate LiCl and the solvent was eliminated from the filtrate under vacuum condition. Fractional distillation was performed at 100 C at 10-2 torr to obtain Sn(btsa)2. Sn(btsa)2 (1 g, 2.28 mmol) was dissolved in normal hexane. 2 Equivalent of dimethylamino-2-methyl-2-propanol (0.53 g, 4.56 mmol) was added thereto slowly at room temperature, followed by stirring for 6 hours. After eliminating the solvent under vacuum condition, fractional distillation was performed at 100C at 10-2 torr to give pure Sn(dmamp)2 compound (91 %). Element analysis for C12H28N2O2Sn-H2O {calculated value (measured value)}: C, 39.05 (37.92); H, 8.19 (7.66); N, 7.59 (8.02) The 1H-NMR of the Sn(dmamp)2 compound prepared in example 1 is shown in Figure 1, the 13C-NMR is shown in Figure 2, and the FT-IR is shown in Figure 3. The TGA and DTA of the Sn(dmamp)2 compound prepared in example 1 are shown in Figure 4. As shown in Figure 4, the (dimethylamino-2-methyl-2-propoxy)Sn(II) [Sn(dmamp)2] compound of the present invention exhibited rapid loss of mass at the temperature range of 300-350 C.
Reference： [1]Patent: EP2105444,2009,A1 .Location in patent: Page/Page column 4
  • 58
  • [ 14123-48-9 ]
  • (dimethylamino-2-methyl-2-propoxy)Sn(II) [ No CAS ]
YieldReaction ConditionsOperation in experiment
With bis(bis(trimethylsilyl)amido)tin(II); In hexane; at 20℃; SnCl2 (1 g, 5.27 mmol) and Lithium bistrimethylsilylamide[Li(btsa)] (1.76 g, 10.54 mmol) were added in 250 mL Schlenk flask at room temperature, to which ether (50 mL) was added, followed by stirring for 3 hours. The mixed solution was filtered to eliminate LiCl and the solvent was eliminated from the filtrate under vacuum condition. Fractional distillation was performed at 100 C. at 10-2 torr to obtain Sn(btsa)2. Sn(btsa)2 (1 g, 2.28 mmol) was dissolved in normal hexane. 2 Equivalent of dimethylamino-2-methyl-2-propanol (0.53 g, 4.56 mmol) was added thereto slowly at room temperature, followed by stirring for 6 hours.After eliminating the solvent under vacuum condition, fractional distillation was performed at 100 C. at 10-2 torr to give pure Sn(dmamp)2 compound (91%).Element analysis for C12H28N2O2Sn.H2O {calculated value (measured value)}: C, 39.05 (37.92); H, 8.19 (7.66); N, 7.59 (8.02).The 1H-NMR of the Sn(dmamp)2 compound prepared in example 1 is shown in FIG. 1, the 13C-NMR is shown in FIG. 2, and the FT-IR is shown in FIG. 3.The TGA and DTA of the Sn(dmamp)2 compound prepared in example 1 are shown in FIG. 4. As shown in FIG. 4, the (dimethylamino-2-methyl-2-propoxy)Sn(II) [Sn(dmamp)2] compound of the present invention exhibited rapid loss of mass at the temperature range of 300-350 C.
Reference： [1]Patent: US2009/275770,2009,A1 .Location in patent: Page/Page column 2
  • 59
  • [ 14123-48-9 ]
  • lead(II) chloride [ No CAS ]
  • 2C6H14NO(1-)*Pb(2+) [ No CAS ]
YieldReaction ConditionsOperation in experiment
38% In a light-protected flask were put 0.478 mol of lead dichloride, 2000 ml of dehydrated diethyl ether, and 0.935 mol of bis(trimethylsilyl)aminolithium and stirred at 25C for 24 hours in a dry argon atmosphere. The diethyl ether solvent was removed by evaporation, and 3000 ml of dehydrated hexane was added to the residue. The solid phase was removed by filtration. To the resulting solution was added dropwise 1.03 mol of <strong>[14123-48-9]1-dimethylamino-2-methyl-2-propanol</strong>, followed by stirring at 25C for 24 hours. Hexane and by-produced hexamethyldisilazane were removed by distillation. From the fraction at 13 to 15 Pa and a tower top temperature of 90 to 95C was obtain white crystals in a yield of 38%, which were further purified by distillation under reduced pressure to obtain crystals. The recovery of the purification was 90%. The resulting crystals were identified to be the title compound, compound No. 1. The analytical values of the crystals were as follows. Results of analyses: (1) Elemental analysis (metal analysis: ICP-AES) Pb: 48.1 % by mass (calcd.: 47.1 %) (2) 1H-NMR (solvent: deuterobenzene) (chemical shift: multiplicity:number of hydrogens) (1.45:s:12) (2.26a:12) (2.56:s:4) (3) TG-DTA (Ar: 100 ml/min; temperature rise: 10C/min; amount of sample: 9.665 mg) Melting point: 61C 50% mass loss temperature: 191C
Reference： [1]Patent: EP1698614,2006,A1 .Location in patent: Page/Page column 7-8
  • 60
  • [ 864757-74-4 ]
  • [ 14123-48-9 ]
  • 4-(benzyloxy)-1-(4-([1-(dimethylamino)-2-methylpropan-2-yl]oxy)phenyl)pyridin-2(1H)-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
61% With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20℃; for 4h; General procedure: To a solution of 4-(4-fluorophenyl)-1-(4-hydroxyphenyl)pyridin-2(1H)-one (12, 40 mg, 0.142 mmol), PPh3 (56 mg, 0.213 mmol), 2-(piperidin-1-yl)ethanol (0.025 mL, 0.170 mmol) in THF (2 mL) was added diethyl azodicarboxylate (37 mg, 0.213 mmol). The mixture was stirred at room temperature for 4 h and concentrated under reduced pressure. The residue was purified by flash chromatography on silica gel (MeOH/CHCl3) and crystallized (EtOAc/hexane) to give compound 5a (41 mg, 73%) as a white solid.
Reference： [1]Bioorganic and Medicinal Chemistry,2011,vol. 19,p. 883 - 893
  • 61
  • [ 877817-57-7 ]
  • [ 14123-48-9 ]
  • [ 19289-58-8 ]
  • [ 67-64-1 ]
Reference： [1]European Journal of Inorganic Chemistry,2011,p. 1833 - 1839
  • 62
  • [ 17973-86-3 ]
  • [ 14123-48-9 ]
  • [ 1360056-82-1 ]
YieldReaction ConditionsOperation in experiment
65% With sodium hydride; In tetrahydrofuran; at 0 - 20℃; Step 1. Preparation of [2-(6-Bromo-pyridazin-3-yloxy)-2-methyl-propyl]-dimethyl-amine In a 100 mL round bottom flask was added <strong>[14123-48-9]1-(dimethylamino)-2-methylpropan-2-ol</strong> (1.48 g, 12.6 mmol, Eq: 1.5), THF and 3,6-dibromopyridazine (2 g, 8.41 mmol, Eq: 1.00). The flask was cooled to 0 C. followed by addition of NaH (572 mg, 14.3 mmol, Eq: 1.7) in one portion. The turbid reaction mixture was allowed to warm to room temperature and was stirred at room temperature overnight. The resultant black reaction mixture was absorbed onto silica gel and purified by LC chromatography eluting with 0-5% MeOH in 1/1 EtOAc/Hex to afford 1.5 g (65%) of the title compound.
Reference： [1]Patent: US2012/40949,2012,A1 .Location in patent: Page/Page column 103
  • 63
  • [ 14123-48-9 ]
  • [ 1149756-76-2 ]
YieldReaction ConditionsOperation in experiment
87% With sodium; In hexane; at 0℃;Reflux; Inert atmosphere; Na(dmamp). dmampH (5.1g, 43.5mmol) was slowly added to a suspension of sodium (1.0g, 43.5mmol) in hexane (50mL) at 0C, and the mixture was allowed to reflux overnight. After cooling to room temperature, the solvent was removed to obtain Na(dmamp) as a white powder (5.3g, 87%). 1H NMR (C6D6, 500MHz): delta 1.23 (s, 6H, OC(CH3)2), 2.24 (s, 8H, N(CH3)2 and CH2).
Reference： [1]Polyhedron,2020,vol. 176
[2]Organometallics,2012,vol. 31,p. 8109 - 8113
[3]Dalton Transactions,2015,vol. 44,p. 2103 - 2109
  • 64
  • [ 14123-48-9 ]
  • [Mg(1-dimethylamino-2-methyl-2-propanol(-H))-(trifluoroacetylacetone(-H))]2 [ No CAS ]
Reference： [1]Dalton Transactions,2015,vol. 44,p. 2103 - 2109
  • 65
  • [ 14123-48-9 ]
  • [ 75-24-1 ]
  • C13H31AlN2O2 [ No CAS ]
Reference： [1]European Journal of Inorganic Chemistry,2015,vol. 2015,p. 2323 - 2329
  • 66
  • [ 14123-48-9 ]
  • [ 75-24-1 ]
  • C16H40Al2N2O2 [ No CAS ]
Reference： [1]European Journal of Inorganic Chemistry,2015,vol. 2015,p. 2323 - 2329
  • 67
  • [ 14123-48-9 ]
  • Bis(1,2-dimethoxyethane-O,O')strontium-bis<bis(trimethylsilyl)amide> [ No CAS ]
  • [Sr(1-(dimethylamino)-2-methylpropan-2-ol)(5-[2-(dimethylamino)ethyl]amino}-2,2,6,6-tetramethylhept-4-en-3-one)]2 [ No CAS ]
Reference： [1]Inorganica Chimica Acta,2015,vol. 436,p. 118 - 122
  • 68
  • [ 14123-48-9 ]
  • [Co(1-dimethylamino-2-methylpropane-2-ol)(1,1,1-trifluoro-2,4-pentanedione)]2 [ No CAS ]
Reference： [1]Patent: KR2017/37102,2017,A
  • 69
  • [ 14123-48-9 ]
  • [Co(1-dimethylamino-2-methylpropane-2-ol)(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)]2 [ No CAS ]
Reference： [1]Patent: KR2017/37102,2017,A
  • 70
  • [ 14123-48-9 ]
  • [Co(1-dimethylamino-2-methylpropane-2-ol)(2,2,6,6-tetramethyl-3,5-heptanedione)]2 [ No CAS ]
Reference： [1]Patent: KR2017/37102,2017,A
  • 71
  • [ 14123-48-9 ]
  • [Co(1-dimethylamino-2-methylpropane-2-ol)(acetylacetone)]2 [ No CAS ]
Reference： [1]Patent: KR2017/37102,2017,A
  • 72
  • [ 14123-48-9 ]
  • [ 18544-54-2 ]
  • [Co(1-dimethylamino-2-methylpropane-2-ol)(bis(trimethylsilyl)amide)]2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
90% In tetrahydrofuran; at -78℃; for 3h;Schlenk technique; Co (btsa) 2 (cobalt bis (bis (trimethylsilyl) amide)) (2.53 g, 6.96 mmol, 1 eq) was added to a Schlenk flask in tetrahydrofuranDimethylamin-2-methylpropan-2-ol (dmampH) (0.81 g, 6.96 mmol, 1Eq) in tetrahydrofuran (10 mL) was added slowly. After stirring at -78 C for 3 hours, the reaction mixture was cooled to room temperature (23 C)The mixture was stirred for an additional 12 hours and then the solvent was removed to obtain a green solid (2.24 g, 90%).
Reference： [1]Patent: KR2017/37102,2017,A .Location in patent: Paragraph 0155-0158
  • 73
  • [ 14123-48-9 ]
  • [ 75-24-1 ]
  • C16H40Al2N2O2 [ No CAS ]
Reference： [1]ChemSusChem,2019,vol. 12,p. 4211 - 4220
  • 74
  • [ 14123-48-9 ]
  • Sb(dmamp)<SUB>3</SUB> [ No CAS ]
Reference： [1]Polyhedron,2020,vol. 176
  • 75
  • [ 14123-48-9 ]
  • Ge(dmamp)<SUB>2</SUB> [ No CAS ]
Reference： [1]Polyhedron,2020,vol. 176
  • 76
  • tin(IV) tert-butoxide [ No CAS ]
  • [ 14123-48-9 ]
  • C20H46N2O4Sn [ No CAS ]
YieldReaction ConditionsOperation in experiment
98% In pentane at 20℃; for 1h; Schlenk technique; Inert atmosphere;
Reference： [1]Daniele, Stéphane; Decams, Jean-Manuel; Guillon, Hervé; Jeanneau, Erwann; Mishra, Shashank; Verchère, Alexandre [Inorganic Chemistry, 2020, vol. 59, # 10, p. 7167 - 7180]
  • 77
  • [ 14123-48-9 ]
  • [ 75-05-8 ]
  • [ 25516-30-7 ]
YieldReaction ConditionsOperation in experiment
45% Stage #1: acetonitrile With sulfuric acid at 0℃; Inert atmosphere; Stage #2: 1-dimethylamino-2-methyl-propan-2-ol In acetonitrile at 0 - 20℃; for 48h;
Reference： [1]Chung, Taek-Mo; Kim, Chang Gyoun; Lee, Ga Yeon; Lee, Sunju; Park, Bo Keun [RSC Advances, 2020, vol. 10, # 50, p. 29659 - 29667]
  • 78
  • [ 14123-48-9 ]
  • [Mn((1-(dimethylamino)-2-methylpropan-2-yl)(ethyl)amide)(NEt2)]2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1.1: sulfuric acid / 0 °C / Inert atmosphere 1.2: 48 h / 0 - 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux 2.2: Inert atmosphere 3.1: n-butyllithium / 12 h / 0 °C 4.1: tetrahydrofuran / 6 h / 20 °C / Inert atmosphere 4.2: 12 h / Inert atmosphere
Reference： [1]Chung, Taek-Mo; Kim, Chang Gyoun; Lee, Ga Yeon; Lee, Sunju; Park, Bo Keun [RSC Advances, 2020, vol. 10, # 50, p. 29659 - 29667]
  • 79
  • [ 14123-48-9 ]
  • Mn((1-(dimethylamino)-2-methylpropan-2-yl)(ethyl)amide)(N,N'-diisopropylacetamidinate) [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1.1: sulfuric acid / 0 °C / Inert atmosphere 1.2: 48 h / 0 - 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux 2.2: Inert atmosphere 3.1: n-butyllithium / 12 h / 0 °C 4.1: tetrahydrofuran / 6 h / 20 °C / Inert atmosphere 4.2: 12 h / Inert atmosphere
Reference： [1]Chung, Taek-Mo; Kim, Chang Gyoun; Lee, Ga Yeon; Lee, Sunju; Park, Bo Keun [RSC Advances, 2020, vol. 10, # 50, p. 29659 - 29667]
  • 80
  • [ 14123-48-9 ]
  • lithium (1-(dimethylamino)-2-methylpropan-2-yl)(ethyl)amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: sulfuric acid / 0 °C / Inert atmosphere 1.2: 48 h / 0 - 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux 2.2: Inert atmosphere 3.1: n-butyllithium / 12 h / 0 °C
Reference： [1]Chung, Taek-Mo; Kim, Chang Gyoun; Lee, Ga Yeon; Lee, Sunju; Park, Bo Keun [RSC Advances, 2020, vol. 10, # 50, p. 29659 - 29667]
  • 81
  • [ 14123-48-9 ]
  • N<SUB>2</SUB>-ethyl-N<SUB>1</SUB>,N<SUB>1</SUB>,2-trimethylpropane-1,2-diamine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: sulfuric acid / 0 °C / Inert atmosphere 1.2: 48 h / 0 - 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Inert atmosphere; Reflux 2.2: Inert atmosphere
Reference： [1]Chung, Taek-Mo; Kim, Chang Gyoun; Lee, Ga Yeon; Lee, Sunju; Park, Bo Keun [RSC Advances, 2020, vol. 10, # 50, p. 29659 - 29667]
  • 82
  • [ 14123-48-9 ]
  • [ 55853-40-2 ]
  • C16H40N4O2Sn2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
71% In hexane for 2h;
Reference： [1]Parish, James D.; Snook, Michael W.; Johnson, Andrew L. [Dalton Transactions, 2021, vol. 50, # 39, p. 13902 - 13914]
  • 83
  • [ 14123-48-9 ]
  • [ 55147-78-9 ]
  • C12H28N2O2Sn [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% In hexane for 2h;
Reference： [1]Parish, James D.; Snook, Michael W.; Johnson, Andrew L. [Dalton Transactions, 2021, vol. 50, # 39, p. 13902 - 13914]
  • 84
  • [ 14123-48-9 ]
  • [ 55147-78-9 ]
  • C12H32N2OSi2Sn [ No CAS ]
YieldReaction ConditionsOperation in experiment
66% In hexane for 2h;
Reference： [1]Parish, James D.; Snook, Michael W.; Johnson, Andrew L. [Dalton Transactions, 2021, vol. 50, # 39, p. 13902 - 13914]

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