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[ CAS No. 1413365-66-8 ] {[proInfo.proName]}

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Chemical Structure| 1413365-66-8
Chemical Structure| 1413365-66-8
Structure of 1413365-66-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1413365-66-8 ]

CAS No. :1413365-66-8 MDL No. :N/A
Formula : C20H13ClN2 Boiling Point : -
Linear Structure Formula :- InChI Key :VWNYQJPJWQSBSL-UHFFFAOYSA-N
M.W : 316.78 Pubchem ID :90017857
Synonyms :

Safety of [ 1413365-66-8 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1413365-66-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1413365-66-8 ]

[ 1413365-66-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1161009-89-7 ]
  • 4-([1,1'-biphenyl]-3-yl)-2-chloroquinazoline [ No CAS ]
  • C45H28N2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide; sodium hydroxide; In water; toluene; at 110℃; for 12h;Inert atmosphere; Compound 1-36-2 (8.8 g, 20 mmol) and Compound 1-44-2 (6.3 g, 20 mmol), tetrakis(triphenylphosphine)palladium (1.15 g, 1 mmol), tetrabutylammonium bromide (1.3 g, 4 mmol), sodium hydroxide (1.6 g, 40 mmol), water (10 mL) and toluene (60 mL) were added to a 150 mL three-necked flask under nitrogen atmosphere, and the solution was heated to 110 C. and reacted under stirring for 12 hours, and then the reaction was ended. The reaction solution was rotary evaporated to remove most of the solvent, and then dissolved with dichloromethane and washed with water for 3 times. The organic solution was collected, mixed with silica gel, and then purified by column chromatography, with a yield of 75%.
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