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Chemical Structure| 1415107-30-0 Chemical Structure| 1415107-30-0

Structure of 1415107-30-0

Chemical Structure| 1415107-30-0

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Product Details of [ 1415107-30-0 ]

CAS No. :1415107-30-0
Formula : C13H16ClNO3
M.W : 269.72
SMILES Code : O=C(OC(C)(C)C)NC1=CC(C(C)=O)=CC=C1Cl

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Application In Synthesis of [ 1415107-30-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1415107-30-0 ]

[ 1415107-30-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1190865-44-1 ]
  • [ 1415107-30-0 ]
  • tert-butyl N-{2-chloro-5-[3-(3,5-dichloro-4-fluorophenyl)-4,4,4-trifluoro-3-hydroxy-butanoyl]phenyl}carbamate [ No CAS ]
YieldReaction ConditionsOperation in experiment
27 g With triethylamine; In tetrahydrofuran; at 60 - 80℃; for 2h; Obtained by Reference Production Example 5 resulting N-(5- acetyl-2-chlorophenyl)carbamic acid tert- butyl 13.5g as in Reference Production Example 7 3', 5'-dichloro-4'-fluoro-2 2,2-trifluoro acetophenone 15.5g and triethylamine14.0mL of tetrahydrofuran 100 mL, 1 h at 60 C, and stirred for 1 hour at 80 C. Cooled to room temperature, the reaction mixture was concentrated underreduced pressure, N-{2-chloro-5- [3- (3,5-dichloro-4-fluorophenyl)-4,4,4-trifluoro-3-hydroxy butanoyl] phenyl} carbamic acid tert- butyl toobtain a crude product 27.0g
 

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